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Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance Based) 用电感耦合等离子体原子发射光谱法分析铝和铝合金的标准试验方法(基于性能)
发布日期: 2024-05-15
1.1 本试验方法描述了以下元素的铝和铝合金的电感耦合等离子体原子发射光谱分析: 元素 应用范围,% 最低限度 最大限度 硅 0.02 16.8 Fe 0.02 3.06 铜 0.005 7 Mn 0.003 1.41 Mg 0.006 8.2 Cr 0.004 0.52 镍 0.004 2.71 Zn 0.02 9.65 Ti 0.009 0.20 Ag 0.003 0.4 像 0.005 0.012 B 0.009 0.027 文学士 0.002 0.03 是 0.002 0.11 Bi 0.01 0.59 Ca 0.003 0.048 Cd 0.002 0.055 有限公司 0.002 0.034 Ga 0.01 0.019 锂 0.001 2.48 钼 0.02 0.15 Na 0.008 0.026 P 0.01 0.025 Pb 0.009 0.51 某人 0.01 0.28 Sc 0.01 0.065 Sn 0.008 6.28 Sr 0.0008 0.028 Ti 0. 005 0.20 Tl 0.009 0.13 五、 0.01 0.12 锆 0.004 0.25 1.2 该试验方法仅针对规定的元素和范围进行了实验室间试验。如果方法验证包括方法灵敏度、精密度和偏差的评估(如第节所述 14 ),执行。此外,验证研究必须使用参考材料或加标回收率,或两者兼而有之,评估样品制备方法的可接受性。用户应根据实验室的数据质量目标仔细评估验证数据。 范围扩展的方法验证也是ISO/IEC 17025的一项要求。 1.3 以国际单位制表示的数值应视为标准。本标准不包括其他计量单位。 1.4 本标准并不旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 安全隐患说明见第节 10 具体的警告声明在第节中给出 15 , 17 , 18 , 19 , 20 和 21 . 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ====意义和用途====== 5.1 本分析铝和铝合金的试验方法主要用于测试材料是否符合美国铝业协会股份有限公司的要求。 5. 铝和铝合金的注册成分限制或其他规定的成分限制。 5.2 假设所有使用该测试方法的人员都是经过培训的分析员,能够熟练、安全地执行常见的实验室程序,并且工作将在设备齐全的实验室中进行。 5.3 这是一种基于性能的测试方法,它更多地依赖于测试结果的证明质量,而不是严格遵守特定的程序步骤。预计使用这种测试方法的实验室将编制自己的工作说明书。这些工作说明应包括特定实验室的详细操作说明、使用的特定参考材料和性能验收标准。
1.1 This test method describes the inductively coupled plasma atomic emission spectrometric analysis of aluminum and aluminum alloys for the following elements: Elements Application Range, % Minimum Maximum Si 0.02 16.8 Fe 0.02 3.06 Cu 0.005 7.0 Mn 0.003 1.41 Mg 0.006 8.2 Cr 0.004 0.52 Ni 0.004 2.71 Zn 0.02 9.65 Ti 0.009 0.20 Ag 0.003 0.4 As 0.005 0.012 B 0.009 0.027 Ba 0.002 0.03 Be 0.002 0.11 Bi 0.01 0.59 Ca 0.003 0.048 Cd 0.002 0.055 Co 0.002 0.034 Ga 0.01 0.019 Li 0.001 2.48 Mo 0.02 0.15 Na 0.008 0.026 P 0.01 0.025 Pb 0.009 0.51 Sb 0.01 0.28 Sc 0.01 0.065 Sn 0.008 6.28 Sr 0.0008 0.028 Ti 0.005 0.20 Tl 0.009 0.13 V 0.01 0.12 Zr 0.004 0.25 1.2 This test method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this test method to other elements or different composition ranges if method validation, which includes evaluation of method sensitivity and precision and bias (as described in Section 14 ), is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. The user should carefully evaluate the validation data against the laboratory’s data quality objectives. Method validation of scope extensions is also a requirement of ISO/IEC 17025. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Safety hazard statements are given in Section 10 and specific warning statements are given in Sections 15 , 17 , 18 , 19 , 20 and 21 . 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method for the analysis of aluminum and aluminum alloys is primarily intended to test material for compliance with The Aluminum Association Inc. 5 registered composition limits or other specified composition limits for aluminum and aluminum alloys. 5.2 It is assumed that all who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely, and that the work will be performed in a properly equipped laboratory. 5.3 This is a performance-based test method that relies more on the demonstrated quality of the test result than on strict adherence to specific procedural steps. It is expected that laboratories using this test method will prepare their own work instructions. These work instructions should include detailed operating instructions for the specific laboratory, the specific reference materials employed, and performance acceptance criteria.
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