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现行 ASTM D5399-09(2023)
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Standard Test Method for Boiling Point Distribution of Hydrocarbon Solvents by Gas Chromatography 用气相色谱法测定烃类溶剂沸点分布的标准试验方法
发布日期: 2023-07-01
1.1 本试验方法包括用毛细管气相色谱法测定烃类溶剂的沸点分布。该试验方法仅限于最小初始沸点为37的样品 °C(99 °F),最大最终沸点为285 °C(545 °F),沸腾范围为5 °C至150 °C(9 °F至270 °F)。 1.2 为了确定使用该测试方法观察或计算的值是否符合相关规范,应将测试结果四舍五入到右上角的“最接近的单位”- 根据实施规程的四舍五入法,用于表示规格极限的手数字 E29 。 1.3 以国际单位制表示的数值是标准值。括号中给出的值仅供参考。 1.4 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ===意义和用途====== 5.1 碳氢化合物溶剂沸点分布的气相色谱测定可作为传统蒸馏方法的替代方法,用于控制制造过程中的溶剂质量和规格测试。 5.2 沸点分布数据可用于监测烃溶剂制造过程中产品污染物的存在和成分变化。 5.3 通过该试验方法获得的沸点分布数据与通过试验方法得到的数据不等效 D86 , D850 , D1078 , 1887年2月 , D2892 和 D3710 。
1.1 This test method covers the determination of the boiling point distribution of hydrocarbon solvents by capillary gas chromatography. This test method is limited to samples having a minimum initial boiling point of 37 °C (99 °F), a maximum final boiling point of 285 °C (545 °F), and a boiling range of 5 °C to 150 °C (9 °F to 270 °F) as measured by this test method. 1.2 For purposes of determining conformance of an observed or calculated value using this test method to relevant specifications, test result(s) shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29 . 1.3 The values stated in SI units are standard. The values given in parentheses are for information purposes only. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 The gas chromatographic determination of the boiling point distribution of hydrocarbon solvents can be used as an alternative to conventional distillation methods for control of solvents quality during manufacture, and specification testing. 5.2 Boiling point distribution data can be used to monitor the presence of product contaminants and compositional variation during the manufacture of hydrocarbon solvents. 5.3 Boiling point distribution data obtained by this test method are not equivalent to those obtained by Test Methods D86 , D850 , D1078 , D2887 , D2892 , and D3710 .
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