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废止 ASTM D5597-94
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Practice for the Preparation of Oil-Based Ink Resin Solutions Using a Hot Oil Bath (Withdrawn 1999) 使用热油浴制备油基油墨树脂溶液的实施规程(1999年撤销)
发布日期: 1994-01-01
1.1本规程涵盖了使用热油浴在高沸点溶剂中制备油基油墨树脂溶液的实验室程序。 1.2本规程使用在正常、设备齐全的实验室中普遍可用的实验室设备。 1.3本规程允许快速制备树脂溶液(通常为30至45分钟),并在惰性气氛下调节最高温度,防止制备过程中随机溶剂损失。 1.4本程序适用于主要用于油基胶印和凸版油墨的油墨树脂。树脂的类型通常包括但不限于C 9 芳香烃树脂、改性双环戊二烯树脂、松香季戊四醇或甘油酯、酚醛改性松香酯、马来酸酐改性松香酯和天然树脂,如gilsonite。 1.5使用的典型高沸点溶剂包括C 12 -C 16 石油馏出物,texanol异丁酸,碱- 精制亚麻籽油、十三醇或上述物质的组合。 1.6为避免火灾或对操作员造成伤害,或两者兼而有之,本程序不适用于低闪点溶剂,如甲苯或二甲苯。根据试验方法D56测定,所用溶剂的最低闪点应为60°C(140°F)。 1.7本标准无意解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全和健康实践,并确定监管限制的适用性。
1.1 This practice covers a laboratory procedure for preparing an oil-based ink resin solution in a high boiling solvent using a hot oil bath. 1.2 This practice uses laboratory equipment generally available in a normal, well equipped laboratory. 1.3 This practice allows rapid resin solution preparation (typically 30 to 45 min) and regulates the maximum temperature under an inert atmosphere, preventing the random solvent loss during preparation. 1.4 The procedure is for use with ink resins intended mainly for oil-based offset and letterpress inks. The types of resins are typically, but not limited to, C 9 aromatic hydrocarbon resins, modified dicyclopentadiene resins, rosin pentaerythritol or glycerin esters, phenolic-modified rosin esters, maleic anhydride-modified rosin esters, and naturally occurring resins such as gilsonite. 1.5 The typical high boiling solvents to be used include C 12 -C 16 petroleum distillates, texanol isobutyrate, alkali-refined linseed oil, tridecyl alcohol, or combinations of the above. 1.6 To avoid fire or injury to the operator, or both, this procedure should not be used with low flash point solvents such as toluene or xylene. The minimum flash point of the solvents used should be 60°C (140°F) as determined by Test Method D56. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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归口单位: D01.37
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