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Standard Guide for Reporting Results of Analysis of Water 报告水分析结果标准指南
发布日期: 2018-08-01
1.1 本指南提供了以完整和系统的方式向实验室客户报告饮用水、废水、工艺水、地下水和地表水等分析的无机和有机结果的指南。 1.2 本指南不涉及细菌和放射学数据的报告。 1.3 列出并定义了用于审查和报告信息的常用数据限定符。客户和实验室的特定要求可以使用其他限定符。本指南不排除使用其他数据限定符。 1.4 本指南讨论了报告低水平数据、潜在错误(I型和II型)和报告低于计算方法检测限且高于分析物的数据的程序和具体问题。 1.5 以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.6 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 4.1 正确使用分析数据需要充分记录所有输入,即样品的来源和历史、执行分析的实验室、分析方法、分析日期、测量的精度和偏差以及相关的质量保证信息。 4.2 为了获得可靠的数据,报告必须完整准确,提供足够的信息来评估数据的质量,并包含记录采样和分析程序的支持信息。 4.3 本指南包含一些通用数据限定符或“标志”,通常由遵循良好实验室实践、政府合同计划的实验室使用,或在商业实验室中找到。这些限定符的示例包括(E)用于估计值,(U)用于分析但未检测到的,以及(B)用于空白中发现的分析物(见 8.11 ). 本指南中包含的限定符应有助于实验室及其客户通过使用标准化限定符更好地相互了解。 4.4 实践 D933 是报告水形成成分(如金属氧化物、酸酐等)的综合实践。
1.1 This guide provides guidelines for reporting inorganic and organic results of analyses of drinking water, waste water, process water, ground water, and surface water, and so forth, to laboratory clients in a complete and systematic fashion. 1.2 The reporting of bacterial and radiological data are not addressed in this guide. 1.3 The commonly used data qualifiers for reviewing and reporting information are listed and defined. Client and laboratory specific requirements may make use of other qualifiers. This guide does not preclude the use of other data qualifiers. 1.4 This guide discusses procedures for and specific problems in the reporting of low level data, potential errors (Type I and Type II), and reporting data that are below the calculated method detection limit and above the analyte. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 4.1 The proper use of analytical data requires adequate documentation of all inputs, that is, the source and history of the sample, laboratory performing the analysis, method of analysis, date of analysis, precision and bias of the measurements, and related quality assurance information. 4.2 In order to have defensible data, the report must be complete and accurate, providing adequate information to evaluate the quality of the data and contain supporting information that documents sampling and analysis procedures. 4.3 This guide contains some of the common data qualifiers or “flags” commonly used by laboratories following the good laboratory practices, the government contract program, or found in the commercial laboratories. Examples of these qualifiers are the use of (E) for estimated value, (U) for analyzed for but not detected, and (B) for analyte was found in the blank (see 8.11 ). The qualifiers included in this guide should help the laboratory and its customers to better understand each other by using standardized qualifiers. 4.4 Practice D933 is a comprehensive practice for reporting water-formed constituents such as metal oxides, acid anhydrides, and others.
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