Standard Test Method for Colorimetric Determination of <emph type="ital">p-tert</emph >-Butylcatechol In Styrene Monomer or AMS (α–Methylstyrene) by Spectrophotometry
用分光光度法测定苯乙烯单体或AMS(α-甲基苯乙烯)中对叔丁基邻苯二酚的比色测定的标准试验方法
1.1
本试验方法适用于测定1 mg/kg至100 mg/kg范围。
1.2
在使用该方法确定试验结果是否符合适用规范时,应根据实践中的四舍五入方法对结果进行四舍五舍五入
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基于表1中的ILS数据,检测限为0.2mg/kg,而定量限为0.8mg/kg。
1.3
以国际单位表示的值应视为标准值。本标准不包括其他计量单位。
1.4
本标准并不旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前建立适当的安全、健康和环境实践,并确定监管限制的适用性。
有关危险的具体说明,请参见第节
9
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1.5
本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。
=====意义和用途======
5.1
本试验方法适用于测定TBC抑制剂的量,既可防止运输和储存过程中的聚合,也可用于内部质量控制。
1.1
This test method is applicable to the determination of residual 4-tertiary-butylcatechol (TBC) in styrene monomer or AMS in the 1 mg/kg to 100 mg/kg range.
1.2
In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice
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. The limit of detection is 0.2 mg/kg while the limit of quantitation is 0.8 mg/kg based on the ILS data in Table 1.
1.3
The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
For specific statements on hazards, see Section
9
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1.5
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
====== Significance And Use ======
5.1
This test method is suitable for determining the quantity of TBC inhibitor, both for the protection against polymerization while in transit and storage, and for internal quality control.