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Standard Test Method for Viscosity of Asphalts by Vacuum Capillary Viscometer 用真空毛细管粘度计测定沥青粘度的标准试验方法
发布日期: 2022-11-01
1.1 本试验方法包括在60℃下用真空毛细管粘度计测定沥青粘合剂表观粘度的程序 °C[140 °F]。它适用于粘度在0.0036至20以上的材料 000 Pa·s[0.036至200以上 000p]。 注1: 该试验方法适用于其他温度,但其精度取决于60℃下沥青粘合剂的测定 °C[140 °F]。 注2: 在本试验条件下,经处理或回收的改性沥青粘合剂或沥青粘合剂通常为非牛顿型。非牛顿沥青粘合剂的表观粘度随剪切速率而变化。当毛细管中的流体为非牛顿流体时,使用该试验方法测定的剪切速率可能无效。在本试验的试验条件下,非牛顿行为的存在可通过使用具有不同粘度的粘度计测量粘度来验证- 大小的毛细管或具有不同的压力头。第节中定义的精度限值 11 可能不适用于非牛顿沥青粘合剂。试验方法 D4957型 可能是测试非牛顿沥青的更适用方法。 1.2 以国际单位制或英寸磅单位表示的数值应单独视为标准值。每个系统中规定的值可能不完全相等;因此,每个系统应独立使用。将两个系统的值合并可能导致不符合标准。 1.3 警告- 汞已被美国环境保护署(EPA)和许多州机构指定为有害物质,可导致中枢神经系统、肾脏和肝脏受损。汞或其蒸气可能对健康有害,并对材料有腐蚀性。处理汞和含汞产品时应谨慎。 有关详细信息,请参阅适用的产品材料安全数据表(MSDS)或安全数据表-http://www.epa.gov/mercury/faq.htm-更多信息。用户应注意,州法律可能禁止在您所在州销售汞、含汞产品或两者。 1.4 本标准的文本引用了提供说明材料的注释和脚注。这些注释和脚注(不包括表和图中的注释和脚注)不应视为本标准的要求。 1.5 本标准并不旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前建立适当的安全、健康和环境实践,并确定监管限制的适用性。 1.6 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《国际标准、指南和建议制定原则决定》中确立的国际公认标准化原则制定的。 =====意义和用途====== 5.1 60℃时的粘度 °C[140 °F]表示流动特性,可用于稀释沥青和沥青粘合剂的规范要求。 注3: 本标准产生的结果质量取决于执行程序的人员的能力以及所用设备的能力、校准和维护。符合规范标准的机构 第3666页 通常认为能够进行合格和客观的测试、取样、检验等。本标准的用户应注意遵守规范 第3666页 单独使用并不能完全确保可靠的结果。可靠的结果取决于许多因素;遵循规范的建议 第3666页 或一些类似的可接受准则提供了评估和控制这些因素的方法。
1.1 This test method covers procedures for the determination of the apparent viscosity of asphalt binder by vacuum capillary viscometers at 60 °C [140 °F]. It is applicable to materials having viscosities in the range from 0.0036 to over 20 000 Pa·s [0.036 to over 200 000 P]. Note 1: This test method is suitable for use at other temperatures, but the precision is based on determinations on asphalt binders at 60 °C [140 °F]. Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The apparent viscosity for non-Newtonian asphalt binders varies with shear rate. When the flow is non-Newtonian in a capillary tube, the shear rate determined using this test method may be invalid. The presence of non-Newtonian behavior for the test conditions of this test can be verified by measuring the viscosity with viscometers having different-sized capillary tubes or with different pressure heads. The defined precision limits in Section 11 may not be applicable to non-Newtonian asphalt binders. Test Method D4957 may be a more applicable method for testing non-Newtonian asphalts. 1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. 1.3 Warning— Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law. 1.4 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 The viscosity at 60 °C [140 °F] characterizes flow behavior and may be used for specification requirements for cutback asphalt and asphalt binders. Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
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