1.1 本试验方法包括在给定的时间和温度条件下测定密封小瓶中包装材料中释放的残留溶剂量，是试验方法的推荐替代方法 第151层 . 1.2 本试验方法涵盖了一种挥发性化合物的定量程序，该挥发性化合物的特性已经确定，并保留在包装材料中。 1.3 分析员应通过对感兴趣的溶剂进行适当的研究来确定该方法的灵敏度和再现性。分析师被转介至实践 第260页 以供指导。 1.4 为了验证未知挥发性化合物的身份或识别未知挥发性化合物，鼓励分析员将气相色谱/质谱、气相色谱-红外光谱或其他合适的技术与本测试方法结合起来。 1.5 由于不同类型样品之间基质/溶剂相互作用的变化，必须根据具体情况确定该测试方法在确定给定保留溶剂浓度时的灵敏度。 1.6 本试验方法不涉及包装材料中总残留溶剂的测定。为此可以采用诸如多个顶部空间提取的技术。分析员可参考GC自动取样系统随附的手册进行指导。 1.7 以国际单位制表示的数值应视为标准。 1.8 本标准并非旨在解决与其使用相关的所有安全问题（如有）。本标准的使用者有责任在使用前制定适当的安全、健康和环境实践，并确定监管限制的适用性。 1.9 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ====意义和用途====== 5.1 本试验方法旨在测量在高温条件下从包装材料中排放的挥发性有机化合物。 5.2 这种测试方法可能有助于开发和制造具有最小残留包装油墨/粘合剂溶剂的包装材料。 5.3 通过使用适当的定性GC检测设备（如质谱仪）代替火焰离子化检测器来修改该程序，可以提供身份未知的挥发性有机物的识别。

1.1 This test method covers determination of the amount of residual solvents released from within a packaging material contained in a sealed vial under a given set of time and temperature conditions and is a recommended alternative for Test Method F151 . 1.2 This test method covers a procedure for quantitating volatile compounds whose identity has been established and which are retained in packaging materials. 1.3 The analyst should determine the sensitivity and reproducibility of the method by carrying out appropriate studies on the solvents of interest. The analyst is referred to Practice E260 for guidance. 1.4 For purposes of verifying the identity of or identifying unknown volatile compounds the analyst is encouraged to incorporate techniques such as gas chromatography/mass spectroscopy, gas chromatography/infrared spectroscopy or other suitable techniques in conjunction with this test method. 1.5 Sensitivity of this test method in the determination of the concentration of a given retained solvent must be determined on a case by case basis due to the variation in the substrate/solvent interaction between different types of samples. 1.6 This test method does not address the determination of total retained solvents in a packaging material. Techniques such as multiple headspace extraction can be employed to this end. The analyst is referred to the manual supplied with the GC-Autosampling system for guidance. 1.7 The values stated in SI units are to be regarded as the standard. 1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method is intended to measure volatile organic compounds that are emitted from packaging materials under high-temperature conditions. 5.2 This test method may be useful in assisting in the development and manufacture of packaging materials having minimal retained packaging ink/adhesive solvents. 5.3 Modification of this procedure by utilizing appropriate qualitative GC detection devices such as a mass spectrometer in place of the flame ionization detector may provide identification of volatile organics of unknown identity.