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现行 ASTM E3142-18a(2023)
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Standard Test Method for Thermal Lag of Thermal Analysis Apparatus 热分析仪器热滞后的标准试验方法
发布日期: 2023-06-01
1.1 该测试方法解决了温度校准对温度变化率的依赖性。该测试方法描述了热分析设备热滞后的确定及其在修改该设备在替代线性温度变化率下获得的温度校准中的应用。 1.2 本试验方法适用但不限于差热分析仪(DTA)、差扫描量热仪(DSC)、热重分析仪(TGA)、热机械分析仪(TMA)和动态机械分析仪(DMA)的温度校准。 1.3 该试验方法仅适用于表明指示温度和温度速率之间存在线性关系的仪器- 改变。 1.4 以国际单位制表示的数值应视为标准。本标准中不包括其他计量单位。 1.5 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.6 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ====意义和用途====== 5.1 不同的测量可能需要不同的温度变化率(例如,试验方法 E698 )。温度校准随温度变化率而变化。设备的已知热滞后的使用可以用于将在一个温度变化率下获得的设备的温度校准与给定应用所需的在另一温度变化率上获得的温度校准进行调节。有关温度校准的调整程序,请参阅 8.1 。 5.2 该测试方法可用于研究、质量保证和规范验收。
1.1 This test method addresses the dependence of temperature calibration on the temperature rate-of-change. This test method describes the determination of the thermal lag of thermal analysis apparatus and its application to the modification of the temperature calibration for that apparatus obtained at alternative linear temperature rates-of-change. 1.2 This test method is applicable, but not limited to, the temperature calibration of differential thermal analyzers (DTAs), differential scanning calorimeters (DSCs), thermogravimetric analyzers (TGAs), thermomechanical analyzers (TMAs), and dynamic mechanical analyzers (DMAs). 1.3 This test method is applicable only to apparatus demonstrating a linear relationship between indicated temperature and temperature rate-of-change. 1.4 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 Differing temperature rates-of-change may be required for different measurements (for example, Test Method E698 ). Temperature calibration changes as a function of temperature rate-of-change. The use of the known thermal lag of an apparatus may be used to adjust the temperature calibration of the apparatus obtained at one temperature rate-of-change with that at another required for a given applications. This adjustment procedure for temperature calibration is described in 8.1 . 5.2 This test method may be used in research, quality assurance, and specification acceptance.
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归口单位: E37.10
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