首页 馆藏资源 舆情信息 标准服务 科研活动 关于我们
现行 ASTM E3203-24a
到馆提醒
收藏跟踪
购买正版
Standard Test Method for Determination of Lead by Inductively Coupled Plasma-Optical Emission Spectroscopy (ICP-OES) 电感耦合等离子体光学发射光谱法(ICP-OES)测定铅的标准试验方法
发布日期: 2024-04-01
1.1 本试验方法规定了使用电感耦合等离子体光学发射光谱法(ICP-OES)分析在建筑物和相关结构中及其周围收集的空气中颗粒物、干燥油漆、土壤、灰尘擦拭和微真空样品铅含量的程序。 1.2 该测试方法应由在ICP-OES的使用、光谱和基质干扰的解释及其校正程序方面经验丰富的分析员使用。 1.3 本试验方法引用了制备空气中颗粒物、干燥油漆、土壤和擦拭物样品的试验溶液以进行分析的具体方法。 1.4 用户有责任确保本测试方法对未经测试矩阵的取样材料的有效性。 1.5 由于合适的ICP-OES仪器的不同品牌和型号之间存在差异,因此未提供详细的操作说明。 相反,分析员应遵循特定仪器制造商提供的说明。该测试方法不涉及不同设备的比较精度或相同品牌和型号的仪器之间的精度。 1.6 本试验方法包含说明性注释,不属于本试验方法强制性要求的一部分。 1.7 以国际单位制表示的数值应视为标准。本标准不包括其他计量单位。 1.7.1 例外 擦拭和微真空取样数据所示的英寸磅和国际单位制应单独视为擦拭和微抽真空取样数据的标准。 1.8 本标准并不旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.9 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ====意义和用途====== 5.1 本试验方法旨在与其他标准一起使用,这些标准涉及在评估或减轻建筑物和相关结构的铅危害期间获得的样本(空气中的颗粒物、擦拭和微真空吸尘产生的灰尘、干燥的油漆碎片和土壤)的收集和制备。 5.2 实验室分析在评估或缓解建筑物和相关结构的铅危害期间获得的样本,应符合规程 E1583 ,或应被具有管辖权的当局颁布的铅分析认可,或两者兼而有之。 注1: 在美利坚合众国,对铅基涂料活动期间收集的样品进行分析的实验室需要获得ISO/IEC 17025和环境保护局颁布的其他要求的认证。 5.3 该试验方法也可用于分析其他环境中的类似样品,如使用指南取样的废物的毒性特征提取物 E1908 如使用EPA SW-846测试方法1311进行分析所制备的。
1.1 This test method specifies a procedure for analysis of airborne particulate, dried paint, soil, and dust wipe and micro-vacuumed samples collected in and around buildings and related structures for lead content using inductively coupled plasma-optical emission spectroscopy (ICP-OES). 1.2 This test method should be used by analysts experienced in the use of ICP-OES, the interpretation of spectral and matrix interferences, and procedures for their correction. 1.3 This test method cites specific methods for preparing test solutions of airborne particulate, dried paint, soil, and wipe samples for analysis. 1.4 It is the user’s responsibility to ensure the validity of this test method for sampling materials of untested matrices. 1.5 No detailed operating instructions are provided because of differences among various makes and models of suitable ICP-OES instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model. 1.6 This test method contains notes that are explanatory and are not part of the mandatory requirements of this test method. 1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.7.1 Exception— The inch-pound and SI units shown for wipe and micro-vacuumed sampling data are to be individually regarded as standard for wipe and micro-vacuumed sampling data. 1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method is intended for use with other standards that address the collection and preparation of samples (airborne particulate, dusts by wipe and micro-vacuuming, dried paint chips, and soils) that are obtained during the assessment or mitigation of lead hazards from buildings and related structures. 5.2 Laboratories analyzing samples obtained during the assessment or mitigation of lead hazards from buildings and related structures shall conform to Practice E1583 , or shall be recognized for lead analysis as promulgated by authorities having jurisdiction, or both. Note 1: In the United States of America, laboratories performing analysis of samples collected during lead-based paint activities are required to be accredited to ISO/IEC 17025 and to other requirements promulgated by the Environmental Protection Agency (EPA). 5.3 This test method may also be used to analyze similar samples from other environments such as toxic characteristic extracts of waste sampled using Guide E1908 as prepared for analysis using EPA SW-846 Test Method 1311.
分类信息
关联关系
研制信息
归口单位: D22.12
相似标准/计划/法规
现行
KS L 2018(2020 Confirm)
유리 중의 납 및 카드뮴 정량 방법
玻璃中铅和镉的测定电感耦合等离子体发射光谱法
2015-10-13
现行
BS ISO 22863-5-2021
Fireworks. Test methods for determination of specific chemical substances-Analysis of lead and lead compounds by inductively coupled plasma spectrometry (ICP)
烟火 测定特定化学物质的试验方法
2021-03-26
现行
GBZ/T 316.2-2018
血中铅的测定第2部分:电感耦合等离子体质谱法
Determination of lead in blood-Part 2:Inductively coupled plasma mass spectrometry method
2018-08-16
现行
GB/T 7731.14-2008
钨铁 铅含量的测定 极谱法和电感耦合等离子体原子发射光谱法
Ferrotungsten - Determination of lead content - The polarographic method and inductively coupled plasma-atomic emission spectrometry
2008-05-13
现行
ISO 22863-5-2021
Fireworks — Test methods for determination of specific chemical substances — Part 5: Analysis of lead and lead compounds by inductively coupled plasma spectrometry (ICP)
焰火.特殊化学物质测定的试验方法.第5部分:用电感耦合等离子体光谱法(ICP)分析铅和铅化合物
2021-03-18
现行
GB/T 8152.13-2017
铅精矿化学分析方法 第13部分:铊量的测定 电感耦合等离子体质谱法和电感耦合等离子体-原子发射光谱法
Methods for chemical analysis of lead concentrates—Part 13:Determination of thallium content—Inductively coupled plasma mass spectrometry and inductively coupled plasma-atomic emission spectrometry
2017-10-14
现行
GB/T 32548-2016
钢铁 锡、锑、铈、铅和铋的测定 电感耦合等离子体质谱法
Steel and iron—Determination of tin, antimony, cerium, lead and bismuth—Inductively coupled plasma mass spectrometric method
2016-02-24
现行
GB/T 24875-2010
畜禽粪便中铅、镉、铬、汞的测定 电感耦合等离子体质谱法
Determination of lead,cadmium,chromium,mercury contents in animal manure - Inductively Coupled Plasma Mass Spectrometry method
2010-06-30
现行
ASTM D7303-23
Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry
用电感耦合等离子体原子发射光谱法测定润滑脂中金属的标准试验方法
2023-07-01
现行
NB/SH/T 0864-2013
润滑脂中金属元素的测定 电感耦合等离子体发射光谱法
Standard test method for determination of metals in lubricating greases by inductively coupled plasma atomic emission spectrometry
2013-06-08
现行
ASTM D7439-21
Standard Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass Spectrometry
用电感耦合等离子体质谱法测定空气颗粒物中元素的标准试验方法
2021-09-01
现行
ASTM C1111-10(2020)
Standard Test Method for Determining Elements in Waste Streams by Inductively Coupled Plasma-Atomic Emission Spectroscopy
通过电感耦合等离子体原子发射光谱法测定废物中的元素的标准测试方法
2020-12-01
现行
SN/T 3510-2013
进出口铅矿中砷、镉、铜、镍、铅、锌的测定 电感耦合等离子体原子发射光谱法
Determination of arsenic、cadmium、copper、nickel、lead、zinc in lead ore for import and export-Inductively coupled plasma atomic emission spctrometric method
2013-03-01
现行
YS/T 461.12-2016
混合铅锌精矿化学分析方法 第12部分:铊量的测定 电感耦合等离子体质谱法和电感耦合等离子体原子发射光谱法
Methods for chemical analysis of lead and zinc bulk concentrates—Part 12:Determination of thallium content—Inductively coupled plasma mass spectrometry and inductively coupled plasma atomic emission spectrometry
2016-07-11
现行
GB/T 4702.15-2016
金属铬 铅、锡、铋、锑、砷含量的测定 等离子体质谱法
Chromium metal—Determination of lead,tin,bismuth,antimony and asenic content—Inductively coupled plasma mass spectrometric method
2016-12-13
现行
SN/T 2938-2011
精制铝箔化学成分的测定 电感耦合等离子体原子发射光谱法测定铅、镉、砷
Determination of chemical composition in refining aluminum foil-Determination of lead,cadmium,arsenic-Inductively coupled plasma atomic emission spectrometric method
2011-05-31
现行
ASTM D4951-14(2019)
Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
用电感耦合等离子体原子发射光谱法测定润滑油中添加剂元素的标准试验方法
2019-12-01
现行
NB/SH/T 0824-2010
润滑油中添加剂元素含量的测定 电感耦合等离子体原子发射光谱法
Standard test method for determination of additive elements in lubricating oils by inductively coupled plasma atomic emission spectrometry
2010-05-01
现行
ASTM C1287-18
Standard Test Method for Determination of Impurities in Nuclear Grade Uranium Compounds by Inductively Coupled Plasma Mass Spectrometry
通过电感耦合等离子体质谱法测定核级铀化合物杂质的标准测试方法
2018-01-01
现行
BS ISO 19976-2-2019
Copper, lead and zinc sulfide concentrates. Determination of cadmium-Acid digestion and inductively coupled plasma atomic emission spectrometric method
铜、铅和硫化锌精矿 镉的测定
2019-07-23