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Optimization of SPE and GC/CI-MS/MS as Analytical Methods for Extaction and Detection of NDMA 固相萃取和GC/CI-MS/MS作为NDMA提取和检测分析方法的优化
发布日期: 2004-11-15
固相萃取(SPE)和气相色谱/质谱仪(GC/MS) N-亚硝基二甲胺(NDMA)的分离和检测方法,以及其他选择 各种水基质中的亚硝胺(饮用水、原水、再生水和 描述了废水处理方法。这项工作是由该基金资助的一个更大项目的一部分 题为“测量NDMA的低成本分析法”的WeaEube基金会 “浓度”,在亚硝胺分析的开发方法中。对NDMA测试的兴趣,a 低ng/L水平下可能的人类致癌物源于最近对 各种水源中的NDMA。文中描述的方法被证明是有效的 在1纳克/升最低检测限或以下对NDMA和其他亚硝胺化合物进行定量 (MDL)。该方法也被证明能准确量化饮用水中的亚硝胺浓度, 二级和三级出水样本具有极好的精度。包括9个参考文献、表格、图表。
A solid phase extraction (SPE) and gas chromatography/mass spectrometer (GC/MS) isolation and detection method for N-nitrosodimethylamine (NDMA), and other selected nitrosamines in various water matrices (potable water, raw source water, reclaimed water, and wastewater) is described. This work was performed as part of a larger project funded by the WateReuse Foundation, entitled "Low Cost Analytical Methods for Measuring NDMA Concentrations," in developing methods for nitrosamine analyses. Interest in testing for NDMA, a probable human carcinogen, at low ng/L levels stems from recent concern over the concentration of NDMA in various water supplies. The method described in this paper was shown to effectively quantify NDMA and other nitrosamine compounds at or below a 1-ng/L minimum detection limit (MDL). This method was also shown to accurately quantify nitrosamine concentrations in potable, secondary and tertiary effluent water samples with excellent precision. Includes 9 references, tables, figures.
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发布单位或类别: 美国-美国给水工程协会
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