This report describes the results of the fourth phase of a program to define and advance the state of the art of leak detection for aboveground storage tanks (ASTs). Three leak detection technologies are examined--passive-acoustic, soil-vapor monitoring, and volumetric--over a wide range of tank types, petroleum fuels, and operational conditions. This study also assesses the applicability of a general leak detection methodology involving multiple tests and product levels as well as determines the integrity of 14 ASTs using two or more test methods. See also related documents Publs 322 and 323.