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Standard Test Method for Total Molybdenum in Fresh Alumina-Base Catalysts 新鲜氧化铝基催化剂中总钼的标准测试方法
发布日期: 2021-06-01
1.1 本试验方法涵盖了氧化铝基催化剂中钼的测定,并在钼浓度为8至18重量时进行了协同试验 %, 以MoO表示 3. . 除钼以外的任何催化剂成分,如铁、钨等,在通过锌汞齐还原剂柱(Jones还原剂)后能够被铁离子或铈离子氧化,都会产生干扰。 1.2 单位- 以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.3 许多含有钼的催化剂还含有其他金属,例如镍,这些金属可能受到美国环保局的监管。请参阅所分析催化剂材料的材料安全数据表。更多信息可在EPA上找到。关于含镍催化剂的更多信息,请参见试验方法 D4481 . 1.4 本标准并非旨在解决与其使用相关的所有安全问题(如有)。 本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 4.1 本试验方法规定了一个程序,通过该程序可以在实验室间或实验室内对催化剂样品进行比较。预计催化剂生产商和用户将发现这种方法的价值。
1.1 This test method covers the determination of molybdenum in alumina-base catalysts and has been cooperatively tested at molybdenum concentrations from 8 to 18 weight %, expressed as MoO 3 . Any component of the catalyst other than molybdenum such as iron, tungsten, etc., which is capable of being oxidized by either ferric or ceric ions after being passed through a zinc-amalgam reductor column (Jones reductor) will interfere. 1.2 Units— The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 Many catalysts that contain molybdenum also contain other metals, nickel for example, that may be regulated by the EPA. Go to the material safety data sheet for the catalyst material being analyzed. More information can be found at EPA.gov. Additional information on nickel containing catalysts can be found in Test Method D4481 . 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 4.1 This test method sets forth a procedure by which catalyst samples can be compared either on an interlaboratory or intralaboratory basis. It is anticipated that catalyst producers and users will find this method of value.
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归口单位: D32.03
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