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Standard Test Method for Thermogravimetric Analysis of Hydraulic Cement 水硬水泥热重分析的标准试验方法
发布日期: 2024-12-01
1.1 该测试方法提供了一种结合了热重分析仪的技术,以确定在惰性气体环境中加热时水硬性水泥的质量变化。该数据可用于确定水硬性水泥粉末中一些矿物学成分的丰度。 1.2 单位- 以SI单位表示的值将被视为标准值。本标准不包括其他计量单位。 1.3 本试验方法适用于水硬性水泥粉。 1.4 本标准的正文是指提供解释材料的注释和脚注。这些注释和脚注(不包括表格和图表中的注释和脚注)不应被视为标准的要求。 1.5 本标准并不旨在解决与其使用相关的所有安全性问题(如果有)。本标准的使用者有责任在使用前建立适当的安全、健康和环境实践并确定法规限制的适用性。 1.6 警告- 新鲜的水硬性水泥混合物是腐蚀性的,长时间接触可能会导致皮肤和组织灼伤。建议使用手套、防护服和护目镜。接触后用大量水清洗接触区域。洗眼至少15分钟。避免将身体暴露在浸透了未硬化材料液相的衣物中。暴露后立即脱掉受污染的衣物。 1.7 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。======意义和用途====== 5.1 本试验方法旨在用于获取、分析和报告从水硬性水泥粉末获得的热重数据。 5.2 如果已知石灰石的碳酸钙含量,本试验方法可用于测定石灰石水泥的碳酸钙含量。 5.3 本试验方法可用于测定水硬性水泥粉的氢氧化钙含量。 5.4 该测试方法可用于确定在特定温度范围内加热水硬性水泥粉末时的质量损失。 5.5 该测试方法可用于在一定条件下定性和定量表征各种硫酸盐矿物组分,包括硫酸钙二水合物、硫酸钙半水合物和同长石。5.6 不同种类的热重分析仪具有不同的配置和控制器。因此,所描述的参数应被视为指南。如果报告中注明了变更,则可以对其进行修改以符合仪器制造商的说明。
1.1 This test method provides a technique incorporating a thermogravimetric analyzer to determine the mass changes of hydraulic cement upon heating in an inert gas environment. The data can be used to determine the abundance of some mineralogical components in hydraulic cement powders. 1.2 Units— The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This test method is applicable to hydraulic cement powders. 1.4 The text of this standard refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 Warning— Fresh hydraulic cementitious mixtures are caustic and may cause burns to skin and tissue upon prolonged exposure. The use of gloves, protective clothing, and eye protection is recommended. Wash contact area with copious amounts of water after contact. Wash eyes for a minimum of 15 min. Avoid exposure of the body to clothing saturated with the liquid phase of the unhardened material. Remove contaminated clothing immediately after exposure. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method is intended for use in acquiring, analyzing, and reporting thermogravimetric data obtained from hydraulic cement powders. 5.2 This test method can be used to determine the calcium carbonate content of cements with interground limestone if the calcium carbonate content of the limestone is known. 5.3 This test method can be used to determine the calcium hydroxide content of hydraulic cement powder. 5.4 This test method can be used to determine the mass loss upon heating hydraulic cement powders within a specific temperature range. 5.5 This test method can be used for qualitative and quantitative characterization, under certain conditions, of various sulfate mineral components including calcium sulfate dihydrate, calcium sulfate hemihydrate, and syngenite. 5.6 Different kinds of thermogravimetric analyzers are available with different configurations and controllers. Therefore, the parameters described should be considered as guidelines. They may be altered to conform to the instrument manufacturer’s instructions, provided the changes are noted in the report.
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归口单位: C01.23
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