BS EN 17053:2018规定了测定微量元素、重金属和重金属的方法 通过电感耦合等离子体质谱（ICP-MS）测定动物饲料中的其他元素。方法 用于萃取后测定萃取液中砷、镉、钴、铜、铁、汞、锰、钼、铅、硒、铊、铀和锌 加压消化。用于测定矿物和饲料中的可萃取铅 应使用叶状硅酸盐（例如高岭石粘土）和硝酸湿消化。描述的方法 适用于配备或不配备额外技术的四极杆仪器 减少分子离子干扰（例如碰撞或反应技术）以及高分辨率 扇区现场系统。该方法在一项由八只动物组成的合作试验中进行了全面的统计测试和评估 饲料样品中的元素有砷、镉、钴、铜、铁、汞、锰、钼、铅、硒、铊、铀和锌。元素 当HORRAT值大于2时（例如汞，见附录a），该方法更适用于 筛查方法，不用于确认目的。高分辨率扇形场ICP-MS不适用 在验证环试验中测试。每个元素的量化极限取决于样本矩阵以及 仪器对于元素Co、Mn、Mo、Pb、Tl、U，其定量限应为0.10 mg/kg 通常情况下，铁和锌元素含量为5.0 mg/kg，而镉元素含量为0.03 mg/kg，汞元素含量为0.04 mg/kg 0.05 mg/kg通常是可以量化的。本标准中描述了每个元件成功测试工作范围的详细信息。 交叉引用:EN ISO 6498EN ISO 3696EN ISO 6497（ISO 6497:2002）ASISO 5725-5购买本文件时可获得的所有当前修改件均包含在购买本文件中。

BS EN 17053:2018 specifies a method for the determination of trace elements, heavy metals and other elements in animal feed by inductively coupled plasma mass spectrometry (ICP-MS). The method is used to determine As, Cd, Co, Cu, Fe, Hg, Mn, Mo, Pb, Se, Tl, U and Zn in the extraction solution after pressurized digestion. For the determination of extractable lead in minerals and feeds containing phyllosilicates (e.g. kaolinite clay) wet digestion with nitric acid should be used. The method described is suitable for use in quadrupole instruments equipped either with or without additional technology to reduce molecular ion interferences (e.g. collision or reaction technologies) as well as in high-resolution sector-field systems.The method was fully statistically tested and evaluated in a collaborative trial comprising eight animal feeding stuff samples for the elements As, Cd, Co, Cu, Fe, Hg, Mn, Mo, Pb, Se, Tl, U and Zn. For elements with a HORRAT value higher than 2 (e.g. mercury, see Annex A) the method is more applicable as a screening method and not for confirmatory purposes. High-resolution sector-field ICP-MS was not tested in the validation ring trial.The limit of quantification for each element is dependent on the sample matrix as well as the instrument. For the elements Co, Mn, Mo, Pb, Tl, U a limit of quantification of 0,10 mg/kg should normally be obtained, for the elements Fe and Zn 5,0 mg/kg, while for Cd 0,03 mg/kg, Hg 0,04 mg/kg and As 0,05 mg/kg should normally be quantifiable.Details on the successfully tested working range for each element are described in this standard.Cross References:EN ISO 6498EN ISO 3696EN ISO 6497 (ISO 6497:2002) ASISO 5725-5All current amendments available at time of purchase are included with the purchase of this document.