Water quality. Determination of volatile organic compounds in water. Method using headspace solid-phase micro-extraction (HS-SPME) followed by gas chromatography-mass spectrometry (GC-MS)
水质 水中挥发性有机化合物的测定 方法采用顶空固相微萃取(HS-SPME)和气相色谱-质谱(GC-MS)法
BS EN ISO 17943:2016 specifies a method for the determination of volatile organic compounds. This comprises, for example, halogenated hydrocarbons, trihalogenated methanes,
gasoline components (such as BTEX, MTBE, and ETBE), naphthalene, 2-ethyl-4-methyl-1,3-dioxolane,
and highly odorous substances like geosmin and 2-methylisoborneol in drinking water, ground water,
surface water, and treated waste water, by means of headspace solid-phase micro-extraction (HS-SPME)
followed by gas chromatography-mass spectrometry (GC-MS). The limit of determination depends on
the matrix, on the specific compound to be analysed, and on the sensitivity of the mass spectrometer.
For most compounds to which this International Standard applies, it is at least 0,01 µg/l. Validation
data related to a concentration range between 0,02 µg/l and 2,6 µg/l have been demonstrated in an
interlaboratory trial. Additional validation data derived from standardization work show applicability
of the method within a concentration range from 0,01 µg/l to 100 µg/l of individual substances. All
determinations are performed on small sample amounts (e.g. sample volumes of 10 ml).This method may be applicable to other compounds not explicitly covered by this International Standard
or to other types of water. However, it is necessary to demonstrate the applicability for each case.Cross References:ISO 3696ISO 5667-1ISO 5667-3ISO 5667-5ISO 8466-1ISO 648ISO 1042ISO 4796-2ISO 10301:1997ISO 11423-1:1997ISO 11423-2:1997ISO 15680:2003DIN 38407-41All current amendments available at time of purchase are included with the purchase of this document.