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现行 BS EN ISO 17943:2016
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Water quality. Determination of volatile organic compounds in water. Method using headspace solid-phase micro-extraction (HS-SPME) followed by gas chromatography-mass spectrometry (GC-MS) 水质 水中挥发性有机化合物的测定 方法采用顶空固相微萃取(HS-SPME)和气相色谱-质谱(GC-MS)法
发布日期: 2016-04-30
BS EN ISO 17943:2016规定了测定挥发性有机化合物的方法。这包括卤代烃、三卤甲烷、, 汽油组分(如BTEX、MTBE和ETBE)、萘、2-乙基-4-甲基-1,3-二氧戊环、, 以及饮用水、地下水中的土工蛋白和2-甲基异龙脑等高气味物质, 通过顶空固相微萃取(HS-SPME)处理地表水和经处理的废水 其次是气相色谱-质谱(GC-MS)。决定的限度取决于 基质、待分析的特定化合物以及质谱仪的灵敏度。 对于本国际标准适用的大多数化合物,其含量至少为0.01µg/l。验证 与浓度范围在0.02µg/l和2.6µg/l之间的数据已在实验室中得到证实 实验室间试验。从标准化工作中获得的其他验证数据显示了适用性 在浓度范围为0.01µg/l至100µg/l的单个物质中使用该方法。全部的 对少量样品(例如10毫升的样品体积)进行测定。本方法可能适用于本国际标准未明确涵盖的其他化合物 或其他类型的水。然而,有必要证明每种情况的适用性。交叉引用:ISO 3696ISO 5667-1ISO 5667-3ISO 5667-5ISO 8466-1ISO 648ISO 1042ISO 4796-2ISO 10301:1997ISO 11423-1:1997ISO 11423-2:1997ISO 15680:2003DIN 38407-41购买本文件时提供的所有当前修订版均包括在内。
BS EN ISO 17943:2016 specifies a method for the determination of volatile organic compounds. This comprises, for example, halogenated hydrocarbons, trihalogenated methanes, gasoline components (such as BTEX, MTBE, and ETBE), naphthalene, 2-ethyl-4-methyl-1,3-dioxolane, and highly odorous substances like geosmin and 2-methylisoborneol in drinking water, ground water, surface water, and treated waste water, by means of headspace solid-phase micro-extraction (HS-SPME) followed by gas chromatography-mass spectrometry (GC-MS). The limit of determination depends on the matrix, on the specific compound to be analysed, and on the sensitivity of the mass spectrometer. For most compounds to which this International Standard applies, it is at least 0,01 µg/l. Validation data related to a concentration range between 0,02 µg/l and 2,6 µg/l have been demonstrated in an interlaboratory trial. Additional validation data derived from standardization work show applicability of the method within a concentration range from 0,01 µg/l to 100 µg/l of individual substances. All determinations are performed on small sample amounts (e.g. sample volumes of 10 ml).This method may be applicable to other compounds not explicitly covered by this International Standard or to other types of water. However, it is necessary to demonstrate the applicability for each case.Cross References:ISO 3696ISO 5667-1ISO 5667-3ISO 5667-5ISO 8466-1ISO 648ISO 1042ISO 4796-2ISO 10301:1997ISO 11423-1:1997ISO 11423-2:1997ISO 15680:2003DIN 38407-41All current amendments available at time of purchase are included with the purchase of this document.
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发布单位或类别: 英国-英国标准学会
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