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Standard Test Method of Analysis of Oil-Soluble Sulfonates by Liquid Chromatography 液相色谱法分析油溶性磺酸盐的标准试验方法
发布日期: 2018-04-01
1.1 本试验方法涵盖了精制和粗天然及合成油溶性磺酸盐产品的分析。树脂(如有)用油相回收,羧酸盐作为磺酸盐回收。 1.2 本试验方法包括测定矿物油、磺酸钠、无机盐、水、碱度或酸度、平均分子量和磺酸钠产品的相对密度。 1.3 本试验方法包括测定矿物油、磺酸盐、水、碱值、平均分子量以及钙、钡、镁和磺酸铵产品的相对密度。 1.4 以国际单位制表示的数值应视为标准值。国际单位制后括号中给出的值仅供参考,不被视为标准值。 1.5 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.6 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 5.1 本试验方法提供了一种测定磺酸盐含量的方法,以及根据磺酸盐含量和平均分子量对天然和合成石油磺酸盐产品进行分类和表征的方法。 通过碱度和无机盐含量测量磺酸钠产品的纯度,通过总碱值测量碱土磺酸盐的储备碱度。
1.1 This test method covers the analysis of refined and crude natural and synthetic oil-soluble sulfonate products. Resins, if present, are recovered with the oil phase and carboxylates are recovered as sulfonates. 1.2 This test method covers the determination of mineral oil, sodium sulfonate, inorganic salts, water, basicity or acidity, average molecular weight, and relative density of sodium sulfonate products. 1.3 This test method covers the determination of mineral oil, sulfonate, water, base number, average molecular weight, and relative density of calcium, barium, magnesium, and ammonium sulfonate products. 1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method provides a means of determining sulfonate content and of classifying and characterizing natural and synthetic petroleum sulfonate products by sulfonate content and average molecular weight. Purity of sodium sulfonate products is measured by basicity and inorganic salt contents and the reserve alkalinity of alkaline earth sulfonates by the total base number.
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归口单位: D02.04.0C
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