1.1 这种自动磨损颗粒分析 2. 在役润滑剂的试验方法描述了使用孔隙堵塞颗粒计数和能量色散X射线荧光（EDXRF）光谱法的组合来定量测定大于四（4）微米的固体颗粒计数以及此类润滑剂中铁（Fe）和铜（Cu）悬浮颗粒的元素含量。 1.2 本试验方法用于测定Fe大于4的悬浮颗粒的元素含量 μm，范围为6 mg/kg至223 mg/kg。大于4的铜悬浮颗粒 μm的范围内测定。 在润滑剂中为5mg/kg至92.4mg/kg。总颗粒数大于4 μm的范围为11 495 颗粒/mL大于4 μm至2 169 500 颗粒/mL大于4 μm。 1.3 本试验方法适用于所有已知在用润滑剂（API I-V组）在任何降解阶段。 1.4 该测试方法采用经验元素间校正方法。 1.5 以国际单位制表示的数值应视为标准。本标准不包括其他计量单位。 1.6 本标准并非旨在解决与其使用相关的所有安全问题（如有）。 本标准的使用者有责任在使用前制定适当的安全、健康和环境实践，并确定监管限制的适用性。 1.7 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ====意义和用途====== 5.1 在许多行业中已经表明，将润滑剂中的小元素或溶解元素材料的信息与悬浮颗粒分离是至关重要的。 在许多情况下，仅提供整体元素分析，其可能无法捕捉到显著磨损甚至机械故障事件。此类事件通常伴随着大颗粒物产量的突然增加，这些颗粒物悬浮在机器的润滑剂中，可以在润滑剂中检测到。这种测试方法专门针对这种颗粒物，这种颗粒物在历史上很难量化。该技术的使用者包括许多军事组织，以及风力涡轮机、核电设施和海上钻井平台的维护人员。

1.1 This automatic wear particle analysis 2 test method for in-service lubricants describes using a combination of pore blockage particle counting and energy dispersive X-ray fluorescence (EDXRF) spectrometry for the quantitative determination of solid particle counts larger than four (4) micrometres, and elemental content of suspended particulate of iron (Fe) and copper (Cu) in such lubricants. 1.2 This test method provides for the determination of the elemental content of suspended particulate of Fe greater than 4 μm in the range of 6 mg/kg to 223 mg/kg. Suspended particulate of copper greater than 4 μm is determined in the range of 3.5 mg/kg to 92.4 mg/kg in the lubricant. Total particle count greater than 4 μm is determined in the range of 11 495 particles/mL greater than 4 μm to 2 169 500 particles/mL greater than 4 μm in the lubricant. 1.3 This test method is applicable to all known in-service lubricants (API Groups I-V) at any stage of degradation. 1.4 This test method uses an empirical inter-element correction methodology. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 It has been shown in many industries that separating information regarding small or dissolved elemental materials in the lubricant from suspended particulate is crucial. In many cases only an overall elemental analysis is provided, which may not capture significant wear or even machinery failure events. Such events are often accompanied by a sudden increase in the production of large particulate, which is suspended in and can be detected in the machinery’s lubricant. This test method specifically targets such particulate, which has historically been difficult to quantify. Users of the technique include numerous military organizations, and maintainers of wind turbines, nuclear power facilities, and offshore rigs.