BS EN 16924:2017描述了测定玉米赤霉烯酮含量的程序 食用植物油，特别是玉米胚芽油，采用以下技术之一:高性能 荧光检测液相色谱法（LC-FLD）或高效液相色谱法 稀释油基本提取后，用串联质谱（LC-MS/MS）进行色谱分析。该方法已在自然污染的玉米胚芽油中验证了玉米赤霉烯酮的含量 61,2微克/千克至515微克/千克[5]。实验室经验[6]表明，该方法也适用于其他植物油，如 大豆（n=5），大豆（n=5），葵花籽油（n=5） 油（n=5）、菜籽油（n=11）和混合油，包括玉米胚芽油（n=3）。然而偶尔， 样品可能会对FLD色谱图造成干扰。在这种情况下，MS/MS的检测是 推荐。交叉引用:EN ISO 3696ISO 3696:1987BS EN ISO 3696:1995 ISO/IEC 17025:2005 Ed 1ISO 5725:1986ISO 5725-2ISO 5725-6:1994EN ISO/IEC 17025（ISO/IEC 17025:2005）ASISO 5725-4:1994ISO 5725-5: 1998ISO 5725-3:1994ISO 5725-1:1994购买本文件时可获得的所有现行修改件均包含在购买本文件中。

BS EN 16924:2017 describes a procedure for the determination of the zearalenone content in edible vegetable oils specifically maize germ oil by either of the following techniques: High performance liquid chromatography with fluorescence detection (LC-FLD) or high performance liquid chromatography with tandem mass spectrometry (LC-MS/MS) after basic extraction of the diluted oil.The method has been validated for zearalenone in naturally contaminated maize germ oil at levels of 61,2 µg/kg to 515 µg/kg [5].Laboratory experiences [6] have shown that this method is also applicable to other vegetable oils such as wheat germ oil (n = 4), sunflower oil (n = 5), pumpkin seed oil (n = 1), soybean oil (n = 5), hemp seed oil (n = 5), rape seed oil (n = 11), and mixed oils including maize germ oil (n = 3). However occasionally, samples can result in interferences in the FLD-chromatograms. In this case, the detection with MS/MS is recommended.Cross References:EN ISO 3696ISO 3696:1987BS EN ISO 3696:1995 ISO/IEC 17025:2005 Ed 1ISO 5725:1986ISO 5725-2ISO 5725-6:1994EN ISO/IEC 17025 (ISO/IEC 17025:2005) ASISO 5725-4:1994ISO 5725-5:1998ISO 5725-3:1994ISO 5725-1:1994All current amendments available at time of purchase are included with the purchase of this document.