1.1
This practice covers handling, mixing, and conditioning procedures that are required to ensure that a representative sample of the liquid petroleum or petroleum product is delivered from the primary sample container or container or both into the analytical apparatus or into intermediate containers.
1.2
Appendix X1
details the background information on the development of Table 1 used in performance testing.
Appendix X2
provides guidance in the acceptance testing for water in crude oil.
Appendix X3
provides a guide for materials of sample containers.
Appendix X4
provides a summary of recommended mixing procedures.
Appendix X5
provides a flow chart for sample container/mixing system acceptance test.
1.3
For sampling procedures, refer to Practices
D4057
(API
MPMS
Chapter 8.1) and
D4177
(API
MPMS
Chapter 8.2). Practice
D5842
(API
MPMS
Chapter 8.4) covers sampling and handling of light fuels for volatility measurement, and
D8009
(API
MPMS
Chapter 8.5).
1.4
It is recommended that the users of this practice perform the tests in Practice
D4177
(API
MPMS
Chapter 8.2) before performing the test in this practice.
1.5
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
====== Significance And Use ======
4.1
Representative samples of petroleum and petroleum products are required for the determination of chemical and physical properties used to establish standard volumes, prices, and compliance with commercial and regulatory specifications. The handling of samples from the time of collection until they are analyzed requires care and effort to maintain their compositional integrity. Samples of high RVP (unstabilized) hydrocarbons are required at many measurement points, for example offshore production, at the outlets of test separators or to allow calibration of a flowmeter. This practice also describes requirements associated with handling and mixing samples held within pressurized cylinders.
4.2
Practice
D4057
(API
MPMS
Chapter 8.1), Practice
D4177
(API
MPMS
Chapter 8.2), Practice
D5854
(API
MPMS
Chapter 8.3), Practice
D5842
(API
MPMS
Chapter 8.4), and Practice
D8009
(API
MPMS
Chapter 8.5). The primary purpose of this suite of standards, is to ensure proper sampling and handling for custody transfer applications. There are a significant number of test methods that may be used to analyze the samples taken by techniques described in API
MPMS
Chapter 8.1 and 8.2. For samples that are taken for test methods outside the general scope of custody transfer covered by this practice, the personnel assigned to take the sample are responsible to refer to the test methods for additional critical information that may impact the sampling process, that is, specific container selection, transport methods, storage times, etc. Those requirements should be found in the appropriate test method.