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Carbon-fibre-reinforced composites — Determination of the resin, fibre and void contents 碳纤维增强复合材料树脂、纤维和空隙含量的测定
发布日期: 2024-07-08
本文件规定了根据树脂、纤维和复合材料的密度以及复合材料中纤维的质量计算碳纤维增强复合材料的树脂、纤维和空隙含量的方法(使用方法A),根据复合材料的厚度计算纤维含量(使用方法B),以及通过微观分析计算体积纤维含量和面积空隙含量(使用方法C)。 方法A规定了用于测定复合材料中纤维质量的三种不同的树脂去除程序(即燃烧程序、在硝酸中消解程序和在硫酸和过氧化氢的混合物中消解程序)。通过考虑复合材料中使用的树脂的可燃性、其分解能力和相关树脂的类型来选择要使用的程序。当存在可防止树脂完全溶解和/或可燃性的填充树脂时,方法A仅具有有限的适用性。 方法B(厚度测量方法)仅适用于由单位面积已知纤维质量的预浸料模制而成的复合材料。 方法C(微观方法)仅适用于具有单向、正交和多向层合板的碳纤维增强复合材料。它也可用作测定芳纶或玻璃纤维增强塑料的面积空隙含量和纤维体积含量的参考,但不适用于织物增强复合材料。

This document specifies methods for calculating the resin, fibre and void contents of a carbon-fibre-reinforced composite from the densities of the resin, the fibre and the composite and the mass of fibre in the composite (using method A), for calculating the fibre content from the thickness of the composite (using method B), and for calculating the fibre content by volume and areal void content through microscopic analysis (using method C).

Method A specifies three different resin removal procedures for the determination of the mass of fibre in the composite (viz a combustion procedure, a procedure by digestion in nitric acid and a procedure by digestion in a mixture of sulfuric acid and hydrogen peroxide). The selection of the procedure to be used is made by considering the combustibility of the resin used in the composite, its ability to decompose and the type of resin concerned. Method A is only of limited applicability when filled resins are present that can prevent complete dissolution and/or combustibility of the resin.

Method B (thickness measurement method) is only applicable to composites moulded from prepregs of known fibre mass per unit area.

Method C (microscopic method) is only applicable to carbon-fibre-reinforced composites with unidirectional, orthogonal and multidirectional laminates. It can also be used as reference for determination of the areal void content and fibre volume content of aramid- or glass-fibre-reinforced plastics, but is not applicable to fabric reinforced composites.

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归口单位: ISO/TC 61/SC 13
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