1.1 本试验方法涵盖使用无转子振荡剪切流变仪在低于固化温度的预定温度下测量固化后动态特性。 1.2 还涵盖了近似“静态固化”的规定固化条件，以尽量减少对固化橡胶化合物动态性能的影响。本试验方法无意取代试验方法 D5289 . 1.3 本标准并非旨在解决与其使用相关的所有安全问题（如有）。本标准的用户有责任在使用前制定适当的安全、健康和环境实践，并确定监管限制的适用性。 1.4 警告- 当在本试验方法的固化部分后冷却时，基于硅酮或氟弹性体的化合物可能具有高水平的热收缩或对模具的粘附性差，导致应变扫描期间滑动。 如果发生这种情况，结果将不可靠。 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒（TBT）委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 5.1 本试验方法用于确定（可硫化）橡胶化合物在选定的应变和频率试验条件下的硫化特性，这些条件对硫化动态性能没有显著影响。在同一试验中，该试验方法还将测量硫化胶在明显低于固化温度的温度下的动态性能。 这些较低的温度测量是必要的，以便更有效地与橡胶产品的使用条件相关。 5.2 本试验方法可用于橡胶制造过程中的质量控制以及含硫化剂的橡胶化合物的研发试验。本试验方法也可用于评估因使用不同的复合成分而产生的固化和动态性能差异。 5.3 有关硫化橡胶动态测试重要性的更多信息，读者可能希望参考指南 D5992 .

1.1 This test method covers the use of a rotorless oscillating shear rheometer for measuring after cure dynamic properties at predetermined temperature(s) below the cure temperature. 1.2 Specified cure conditions that approximate a “static cure” also are covered to minimize effects on cured rubber compound dynamic properties. This test method is not intended to replace Test Method D5289 . 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 Warning— Compounds based on silicone or fluoroelastomers may have high levels of thermal contraction or poor adhesion to the dies when cooled after the cure portion of this test method, causing slippage during strain sweeps. If this occurs, the results will not be reliable. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method is used to determine the vulcanization characteristics of (vulcanizable) rubber compounds under selected test conditions of strain and frequency which do not significantly affect the cured dynamic properties. In the same test, this test method also will measure the dynamic properties of the vulcanizate at temperatures significantly below the cure temperature. These lower temperature measurements are necessary in order to more effectively relate to rubber product service conditions. 5.2 This test method may be used for quality control in rubber manufacturing processes and for research and development testing of rubber compounds containing curatives. This test method also may be used for evaluating cure and dynamic property differences resulting from the use of different compounding ingredients. 5.3 For additional information regarding the significance of dynamic testing of vulcanized rubber, the reader may wish to reference Guide D5992 .