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现行 ASTM D8149-20
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Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants 离子色谱测定石油产品和润滑油中杂原子和阴离子的优化 校准和验证的标准实践
发布日期: 2020-07-01
1.1 本规程涵盖了使用离子色谱法(IC)进行阴离子测量的校准、质量控制和操作指南信息。 1.2 IC相关标准- 水基质的化学或电解再生抑制离子色谱标准包括试验方法 D2988 , D4327 , D5085 , D5542 , D5827 , D5987 , D5996 , D6581 , D7319 , D7328 , D7359 , D7773 , D7994 和 D8150 ; 实践中描述了IC仪表要求 E1151 和 E1511 . 1.3 以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.4 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 7.1 对石油产品和润滑剂进行准确的元素分析是确定化学性质的必要条件,化学性质用于确定是否符合商业和监管规范。 7.2 离子色谱法通常用于需要材料阴离子含量的情况。在离子色谱测定之前,一些杂原子可以在氧气环境中燃烧,然后水溶解,将其转化为阴离子。第节列出了许多发布的离子色谱ASTM标准 2. . 其中,使用离子色谱法的D02、D05和D16委员会标准列于 表1 .
1.1 This practice covers the information on calibration, quality control, and operational guidance for anionic measurements using ion chromatography (IC). 1.2 IC Related Standards— Chemically or electrolytically regenerated suppressed ion chromatography standards for aqueous matrices include Test Methods D2988 , D4327 , D5085 , D5542 , D5827 , D5987 , D5996 , D6581 , D7319 , D7328 , D7359 , D7773 , D7994 , and D8150 ; IC instrumentation requirements are described in Practices E1151 , and E1511 . 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 7.1 Accurate elemental analysis of petroleum products and lubricants is necessary for the determination of chemical properties, which are used to establish compliance with commercial and regulatory specifications. 7.2 Ion chromatography is often used in cases where anion content of the material is desired. Some of the hetero-atoms can be converted by combustion in an oxygen atmosphere followed by aqueous dissolution to convert them into anions before ion chromatographic determination. A number of ion chromatographic ASTM standards issued are listed in Section 2 . Of these, the D02, D05, and D16 Committee standards which use ion chromatography are listed in Table 1 .
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归口单位: D02.03
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