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Standard Test Method for Solvents Analysis in Hazardous Waste Using Gas Chromatography 用气相色谱法分析危险废物中溶剂的标准试验方法
发布日期: 2022-03-01
1.1 本试验方法用于使用气相色谱法定性和定量测定废物样品中是否存在以下化合物。本试验方法旨在用作典型报告水平为0.1的筛选方法 %. 二氟甲烷 四氢呋喃 三氯氟甲烷 丙酮 1,1,2-三氯-1,2,2- 三氟乙烷 甲乙酮 MIBK公司 甲醇 环己酮 乙醇 乙酸乙酯 异丙醇 乙酸丙酯 n -丙醇 乙酸丁酯 异丁醇 苯 n -丁醇 甲苯 tert公司 -丁醇 乙苯 二氯甲烷 二甲苯 氯仿 苯乙烯 四氯化碳 氯苯 1,1-二氯乙烷 二氯苯 1,2-二氯乙烷 硝基苯 1,2-二氯丙烷 氟苯 1,1-二氯乙烯 n -丙苯 1,2-二氯乙烯 异丙苯 1,1,1-三氯乙烷 异丁苯 四氯乙烯 n -丁苯 三氯乙烯 2-乙氧基乙醇 四氯乙烷 2-丁氧基乙醇 环戊烷 2-乙氧基乙醇醋酸盐 戊烷 2-甲氧基乙醇 己烷 溴仿 庚烷 卡宾醇 环己烷 乙醚 Iso 辛烷值 1,4-二氧六环 硝基丙烷 二丙酮醇 乙醇胺 乙腈 硝基甲烷 吡啶 氯乙烯 甲苯胺 氯化苄 乙二醇 丙二醇 1.1.1 该化合物列表是危险溶剂和危险废物样品中常见的其他成分的汇编。 1.2 本试验方法的范围可以扩大到包括其他挥发性和半挥发性有机成分,如但不限于以下所述,前提是预期用途数据质量目标(包括采样、回收和分析数据质量)证明用户满意。 1.2.1 碳氢化合物混合物,如煤油和矿物油。 1.2.2 高沸点有机物,此处定义为在上述温度下沸腾的化合物 n -十六烷。 1.2.3 分析员能够通过保留时间数据或气相色谱/质谱(GC/MS)分析识别的其他有机物。 1.3 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.4 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 5.1 本试验方法有助于识别危险废物样品中的常见溶剂成分。本测试方法旨在支持现场或现场评估、回收操作、工厂操作或污染控制计划。
1.1 This test method is used to determine qualitatively and quantitatively the presence of the following compounds in waste samples using gas chromatography. This test method is intended for use as a screening method with a typical reporting level of 0.1 %. Dichodifluoromethane Tetrahydrofuran Trichlorofluoromethane Acetone 1,1,2-Trichloro-1,2,2- trifluoroethane Methyl Ethyl Ketone MIBK Methanol Cyclohexanone Ethanol Ethyl Acetate Isopropanol Propyl Acetate n -Propanol Butyl Acetate Isobutanol Benzene n -Butanol Toluene tert -Butanol Ethylbenzene Methylene Chloride Xylenes Chloroform Styrene Carbon Tetrachloride Chlorobenzene 1,1-Dichloroethane Dichlorobenzenes 1,2-Dichloroethane Nitrobenzene 1,2-Dichloropropane Fluorobenzene 1,1-Dichloroethylene n -Propyl Benzene 1,2-Dichloroethene Isopropyl Benzene 1,1,1-Trichloroethane Isobutyl Benzene Tetrachloroethylene n -Butyl Benzene Trichloroethylene 2-Ethoxyethanol Tetrachloroethane 2-Butoxyethanol Cyclopentane 2-Ethoxyethanol Acetate Pentane 2-Methoxyethanol Hexane Bromoform Heptane Carbitol Cyclohexane Ethyl Ether Iso octane 1,4-Dioxane Nitropropane Diacetone Alcohol Ethanolamine Acetonitrile Nitromethane Pyridine Ethylene Chloride Toluidine Benzyl Chloride Ethylene Glycol Propylene Glycol 1.1.1 This compound list is a compilation of hazardous solvents and other constituents that are commonly seen in hazardous waste samples. 1.2 The scope of this test method may be expanded to include other volatile and semivolatile organic constituents such as but not limited to those described below, provided the intended use data quality objectives including sampling, recovery, and analytic data quality are demonstrated as satisfied by the user. 1.2.1 Hydrocarbon mixtures such as kerosene and mineral spirits. 1.2.2 High-boiling organics, defined here as compounds which boil above n -Hexadecane. 1.2.3 Other organics that the analyst is able to identify, either through retention time data or gas chromatography/mass spectrometric (GC/MS) analysis. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method is useful in identifying the common solvent constituents in hazardous waste samples. This test method is designed to support field or site assessments, recycling operations, plant operations, or pollution control programs.
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归口单位: D34.01.06
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