1.1
This test method covers the determination of dissolved and total recoverable molybdenum in most waters, wastewaters, and brines by atomic absorption spectroscopy.
2
1.2
This test method is applicable in the range from 1 to 25 μg/L of molybdenum. The range may be extended by dilution of the sample.
1.3
This test method has been used successfully with natural and reagent waters. It is the user's responsibility to ensure the validity of this test method for waters of untested matrices.
1.4
The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversion to inch-pound units that are provided for information only and are not considered standard.
1.5
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
For specific precautionary statements, see
8.16
and
11.12
.
1.6
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
====== Significance And Use ======
5.1
Molybdenum can be found in waste that results from chemical cleaning of components in which the metal is alloyed.
5.2
National Pollution Discharge Elimination System (NPDES) permits or other standards, or both, require monitoring pollutants in waste discharged onto the water shed of, or into, navigable waters, and those disposed of in such a manner that eventual contamination of underground water could result.
5.3
This test method affords an accurate and sensitive means of determining compliance with those permits.
5.4
ICP-MS or ICP-AES may also be appropriate but at a higher instrument cost. See Test Methods
D5673
and
D1976
.