目前可用的分析水中卤乙酸（HAAs）和酮酸的方法通常需要使用重氮甲烷进行样品衍生。本文提出了一种基于毒性较小的替代甲基化剂的方法。本研究的目的是开发和评估用于HAA分析的液-液微萃取酸性甲醇衍生程序和用于酮酸分析的微萃取PFBHA酸性甲醇衍生程序。包括23个参考文献、表格和图表。

Currently available methods for analyzing haloacetic acids (HAAs) and ketoacids in water generally require the use of diazomethane for sample derivatization. This article proposes methods based on a less toxic, alternative methylating agent. The objectives of this study were to develop and evaluate a liquid-liquid microextraction-acidic methanol derivatization procedure for HAA analysis and a microextraction-PFBHA-acidic methanol derivatization procedure for ketoacid analysis. Includes 23 references, tables, figures.