本技术规范规定了通过气相色谱质谱（GC-MS）测定谷物类产品中的丙烯酰胺，马铃薯产品和咖啡的方法。 该方法已经通过分析加标样品（炸薯条（未煮过）），面包，水饼干，婴儿谷物，饼干，绿咖啡，烘焙咖啡和速溶咖啡，从30 ug/kg到1500Îg/kg丙烯酰胺。 单个实验室验证的结果由具有丙烯酰胺分析经验的实验室获得。此外，该方法还通过实验室间试验，通过对含有丙烯酰胺的样品的分析进行了研究，范围为约200μg/ kg至2,000μg/ kg。方法的关键点在7.5和条款8中进行了确定

This Technical Specification specifies a method for the determination of acrylamide in cereal-based products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS). The method has been single-laboratory validated via the analysis of spiked samples (French fries (uncooked), bread, water biscuit, infant cereal, biscuit, green coffee, roast coffee and instant coffee), ranging from 30 μg/kg to 1 500 μg/kg acrylamide. The results from the single laboratory validation were obtained by a laboratory with significant experience in acrylamide analysis. In addition, this method has also been studied by inter laboratory trial via the analysis of samples containing incurred acrylamide, ranging from approximately 200 μg/kg to 2 000 μg/kg. Critical points of the method are identified in 7.5 and Clause 8.