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Rubber. Analysis by pyrolytic gas-chromatographic methods-Identification of polymers (single polymers and polymer blends) 橡胶热解气相色谱法分析
发布日期: 2020-03-02
警告1-使用本文件的人员应熟悉正常的实验室实践。本文件并非旨在解决与其使用相关的所有安全问题(如有)。用户有责任建立适当的安全和健康实践,并确定任何其他限制的适用性。 警告2——本文件中规定的某些程序可能涉及使用或产生可能构成当地环境危害的物质,或产生废物。使用后,应参考有关安全处理和处置的适当文件。本文件规定了从相同条件下获得的热解图(热解气相色谱图)中识别原橡胶和硫化或未硫化化合物中的聚合物或聚合物混合物的方法。这允许对单一橡胶或混合橡胶进行定性识别,以下讨论的例外情况除外。 本文件不用于定量分析。 该方法首先适用于单一聚合物。当热解图显示特征碳氢化合物时,该方法也适用于混合物。详情见第5条。当分析员在每个特定情况下进行验证时,该方法也适用于其他类型的聚合物。 注:本文件的使用前提是对气相色谱原理和技术有足够的工作知识,以使分析员能够执行所述操作并正确解释结果。交叉引用:ISO 1629:2013ISO 1407:2011购买本文件时可获得的所有现行修订均包含在购买本文件中。
WARNING 1 — Persons using this document should be familiar with normal laboratory practice. This document does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to determine the applicability of any other restrictions. WARNING 2 — Certain procedures specified in this document might involve the use or generation of substances, or the generation of waste, that could constitute a local environmental hazard. Reference should be made to appropriate documentation on safe handling and disposal after use.This document specifies a method for the identification of polymers, or blends of polymers, in raw rubbers and in vulcanized or unvulcanized compounds from pyrograms (pyrolysis-gas chromatographic patterns) obtained under the same conditions. This allows qualitative identification of single rubbers or blends, with exceptions discussed below. This document is not intended for quantitative analysis. The method applies first and foremost to single polymers. When the pyrogram indicates a characteristic hydrocarbon, the method is also applicable to blends. For details, see Clause 5. The method can be also applicable to other types of polymer when verified by the analyst in each particular case. NOTE The use of this document pre-supposes sufficient working knowledge of the principles and techniques of gas chromatography to enable the analyst to carry out the operations described and to interpret the results correctly.Cross References:ISO 1629:2013ISO 1407:2011All current amendments available at time of purchase are included with the purchase of this document.
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发布单位或类别: 英国-英国标准学会
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