Standard Test Method for Thermal Flow, Cure, and Behavior Properties of Pourable Thermosetting Materials by Torque Rheometer
通过扭矩流变仪测量可浇注热固性材料的热流动 固化和行为性能的标准测试方法
1.1
This test method covers the apparatus, and a specific test method, including the evaluation of results required for the determination of the thermal flow and cure behavior properties of pourable thermosetting materials.
1.2
This test method can be used:
1.2.1
As a control for the development and production of pourable thermosetting materials and to measure the different properties (for example, melting behavior, cure behavior, etc.) as well as the influence of various additives and fillers in any given formulations, and
1.2.2
Verify the uniformity of different production batches of the same formulation.
1.3
The values are stated in SI units.
1.4
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Specific precautions are given in Section
7
.
Note 1:
This standard is equivalent to the inactive ISO 15062. This standard and ISO 15252-2 address the same subject matter, but differ in technical content.
1.5
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
====== Significance And Use ======
5.1
The continuous recording of torque and temperature while going through these various stages can be used to predict the behavior of the material during processing.
5.2
The torque rheometer test has two important functions. First, it is a means to predict flow/viscosity and cure characteristics of pourable thermosetting compounds. For example, the test provides useful data to predict the processibility of a material in a particular molding method. This information is also useful to optimize process conditions for a particular material such as the minimum pressure to fill a mold and the time to cure a part. A second capability of the test is to provide a graphic record of the batch-to-batch uniformity of the molding compound.