Foodstuffs. Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)
食品 气相色谱-质谱法测定食品和咖啡中的丙烯酰胺
发布日期:
2017-08-25
BS PD CEN/TS 17083:2017规定了谷物中丙烯酰胺的测定方法
通过气相色谱-质谱(GC-MS)分析产品、土豆制品和咖啡。通过对加标样品(薯条)的分析,该方法已在单个实验室得到验证
(生的)、面包、水饼干、婴儿麦片、饼干、青咖啡、烤咖啡和速溶咖啡),
范围为30微克/千克到1500微克/千克丙烯酰胺。单个实验室验证的结果由一个具有显著
有丙烯酰胺分析经验。此外,实验室间也对该方法进行了研究
通过分析含有大约200µg/kg丙烯酰胺的样品进行试验
至2000微克/千克。该方法的关键点见7.5和第8条。交叉引用:ISO 3696:1987EN ISO 3696:1995ISO/IEC 5725-
2:1994ISO 1042:1998EN ISO 1042(采用ISO 1042:1998)2002/657/e购买本文件时提供的所有现行修订版均包含在购买本文件中。
BS PD CEN/TS 17083:2017 specifies a method for the determination of acrylamide in cereal-based
products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS).The method has been single-laboratory validated via the analysis of spiked samples (French fries
(uncooked), bread, water biscuit, infant cereal, biscuit, green coffee, roast coffee and instant coffee),
ranging from 30 µg/kg to 1 500 µg/kg acrylamide.The results from the single laboratory validation were obtained by a laboratory with significant
experience in acrylamide analysis. In addition, this method has also been studied by inter laboratory
trial via the analysis of samples containing incurred acrylamide, ranging from approximately 200 µg/kg
to 2 000 µg/kg. Critical points of the method are identified in 7.5 and Clause 8.Cross References:ISO 3696:1987EN ISO 3696:1995ISO/IEC 5725-2:1994ISO 1042:1998EN ISO 1042 (ISO 1042:1998 Adopted)2002/657/ECAll current amendments available at time of purchase are included with the purchase of this document.