Water quality — Determination of polycyclic aromatic hydrocarbons (PAH) — Part 1: Determination of six PAH by high-performance thin-layer chromatography with fluorescence detection after liquid-liquid extraction
水质与灰分;多环芳烃(PAH)的测定第1部分:液-液萃取后荧光检测高效薄层色谱法测定六种多环芳烃
发布日期:
2005-06-27
ISO 7981-1:20 05规定了饮用水中六种选定多环芳烃(PAH)的测定。这6种多环芳烃是:荧蒽、苯并[b]荧蒽、苯并[a]芘、苯并[k]荧蒽、茚并[1,2,3-cd]芘和苯并[ghi]苝
所描述的筛选方法(方法A)排除了那些含有低于20%参考限值的样品。
所述定量方法(方法B)的工作范围为40ng/l至240ng/l(6PAH之和)。可以通过使用较小的样品等分试样来测定较高浓度。
经过一些修改,该方法也适用于地下水和中度污染地表水的分析。
ISO 7981-1:2005 specifies the determination of six selected polycyclic aromatic hydrocarbons (PAH) in drinking water. The 6 PAH are: fluoranthene, benzo[b]fluoranthene, benzo[a]pyrene, benzo[k]fluoranthene, indeno[1,2,3-cd]pyrene, and benzo[ghi]perylene
The screening method (method A) described excludes those samples containing less than 20 % of the referenced limit values.
The quantitative method (method B) described has a working range of 40 ng/l to 240 ng/l (sum of 6 PAH). Higher concentrations may be determined by using a smaller aliquot of the sample.
With some modifications, this method is also applicable for the analysis of ground waters and moderately polluted surface waters.