1.1 This test method describes a bench procedure to simulate the oil aging encountered in Test Method
D7320
, the Sequence IIIG engine test method. These aged oils are then tested for kinematic viscosity and for low-temperature pumpability properties as described in the Sequence IIIGA engine test, Appendix X1 of Test Method
D7320
.
1.2
Units—
The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1
Exceptions—
There are no SI equivalents for some apparatus in Section
6
, and there are some figures where inch units are to be regarded as standard.
1.3
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Specific warning statements are given in Sections
7
and
8
.
1.4 This test method is arranged as follows:
Section
Scope
1
Reference Documents
2
Terminology
3
Summary of Test Method
4
Significance and Use
5
Apparatus
6
Reagents and Materials
7
Hazards
8
Reference Oil Testing and Test Stand Calibration
9
Procedure
10
Cleaning
11
Calculations and Determination of Test Results
12
Report
13
Precision and Bias
14
Keywords
15
Annexes
Reaction Vessel
Annex A1
Reaction Vessel Head
Annex A2
Reaction Vessel-to-Head Seal
Annex A3
Agitator Turbine Blade
Annex A4
Agitator Packing Gland
Annex A5
Nitrogen Dioxide Graduated Tube
Annex A6
Vacuum System Plumbing
Annex A7
Vacuum Trap Condensers
Annex A8
Setting the Vacuum Control Valve
Annex A9
Appendixes
Sample Preparation and Addition
Appendix X1
Charging the Liquid Nitrogen Dioxide
Appendix X2
Nitrogen Dioxide Precision Needle Valve
Appendix X3
Example of an Assembled ROBO Apparatus
Appendix X4
Information Package to Aid Setting Up a New Robo Apparatus
Appendix X5
====== Significance And Use ======
5.1 This bench test method is intended to produce comparable oil aging characteristics to those obtained with ASTM TMC Sequence IIIGA matrix reference oils 434, 435 and 438 after aging in the Sequence IIIG engine test.
5.2 To the extent that the method generates aged oils comparable to those from the Sequence IIIG engine test, the measured increases in kinematic and MRV viscosity indicate the tendency of an oil to thicken because of volatilization and oxidation, as in the Sequence IIIG and IIIGA (see Appendix X1 in Test Method
D7320
) engine tests, respectively.
5.3 This bench test procedure has potential use in specifications and classifications of engine lubricating oils, such as Specification
D4485
.