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现行 ASTM D7741/D7741M-23
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Standard Test Method for Measurement of Apparent Viscosity of Asphalt-Rubber or Other Asphalt Binders by Using a Rotational Handheld Viscometer 用旋转手持粘度计测量沥青橡胶或其他沥青粘合剂表观粘度的标准试验方法
发布日期: 2023-12-01
1.1 在美国和世界范围内,像沥青橡胶这样的高粘度沥青粘合剂的使用越来越普遍。规范,如规范 D6114/D6114M 注意需要现场控制表观粘度,并需要使用现场生产旋转粘度计。沥青橡胶热拌料和沥青橡胶膜中使用的沥青橡胶粘合剂的测试是必要的,以确保混合料性能的一致性,从而确保这些材料的良好性能。现场应用的后勤限制了传统实验室控制和测试设备的使用。该试验使用手持式旋转粘度计,可在现场或实验室进行,以确定沥青橡胶和其他高粘度粘合剂的表观粘度,用于现场生产控制,并评估所生产粘合剂的均匀性,或用于其他相关目的。 1.2 沥青橡胶粘合剂由规范中所述的铺路级沥青水泥和碎橡胶的混合物组成 D6114/D6114M 其他高粘度沥青粘合剂可由用聚合物或纤维或两者改性的沥青组成。在生产过程中,如果有规定的反应时间,则在该反应时间后进行测试。原材料的控制与试验是分开的。 1.3 以国际单位制或英寸磅单位表示的数值应单独视为标准。每个系统中规定的值可能不是完全相等的;每个系统应独立使用。将两个系统的值组合在一起可能会导致不符合标准。 1.4 本标准的文本引用了提供解释性材料的注释和脚注。这些注释和脚注(不包括表和图中的注释和脚注)不应被视为本标准的要求。 1.5 本标准并不旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.6 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ====意义和用途====== 3.1 本试验主要用于沥青橡胶(A-R)和其他高粘度粘合剂的现场生产控制;然而,该测试也可以在实验室环境中使用。 3.2 手持式旋转粘度计用于测量A-R或高粘度粘合剂的完整混合物的表观粘度。将以恒定速度转动的转子(主轴)插入待测量的液体粘合剂中。使用特殊机构测量由周围液体的粘度引起的主轴运动阻力(扭矩),以获得Pa·s或cP的直接读数。 注1: 主轴通常由不锈钢制成,但也可以使用黄铜等其他金属。 3.3 测量的表观粘度用于控制A-R或其他高粘度粘合剂的生产,以评估所生产的粘合剂的均匀性,或用于其他相关目的。 3.4 当心轴在A-R或其他高粘度粘合剂中转动时,它有“钻”入样品的趋势(即,对于A- R、 心轴将橡胶颗粒旋出测量区域)。因此,表观粘度下降以仅反映高粘度粘合剂的液相。因此,记录峰值粘度测量值以反映混合材料的粘度。
1.1 The use of high-viscosity asphalt binders like asphalt-rubber is becoming more common in the United States and worldwide. Specifications such as Specification D6114/D6114M note the need for field control of the apparent viscosity and require the use of a field production rotational viscometer. The testing of asphalt-rubber binder for use in asphalt-rubber hot mix and for asphalt-rubber membrane is necessary to ensure consistent mix properties that will ensure good performance of these materials. Logistics of field applications limits the use of conventional laboratory controls and testing equipment. This test, using a handheld rotational viscometer, can be conducted in either the field or laboratory to determine the apparent viscosity of asphalt-rubber and other high-viscosity binders for field production control and to assess the uniformity of the binder produced, or for other related purposes. 1.2 Asphalt-rubber binder consists of a blend of paving grade asphalt cement and crumb rubber as described in Specification D6114/D6114M . Other high-viscosity asphalt binders may consist of asphalts modified with polymer or fiber, or both. Testing is performed following the specified reaction time, if any, within the production process. Control of the raw materials is separate from the test. 1.3 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; each system shall be used independently of the other. Combining values from the two systems may result in noncompliance with the standard. 1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 3.1 This test is primarily used for field production control of asphalt-rubber (A-R) and other high-viscosity binders; however, the test can also be used in a laboratory setting. 3.2 A handheld rotational viscometer is used to measure the apparent viscosity of a completed blend of A-R or high-viscosity binder. A rotor (spindle), turning at constant speed, is inserted in the liquid binder to be measured. The resistance to movement of the spindle (torque) caused by the viscosity of the surrounding liquid is measured using a special mechanism to obtain direct readings in Pa·s or cP. Note 1: Spindle is generally made of stainless steel, although another metal such as brass could be used. 3.3 The measured apparent viscosity is used to control the production of the A-R or other high-viscosity binder, to assess the uniformity of the binder produced, or for other related purposes. 3.4 As the spindle turns in the A-R or other high-viscosity binder, it has a tendency to “drill” into the sample (that is, for A-R, the spindle spins the rubber particles out of the measurement area). Consequently, the apparent viscosity drops to reflect only the liquid phase of the high-viscosity binder. Therefore, the peak viscosity measurement value is recorded to reflect the viscosity of the blended material.
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归口单位: D04.44
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