美国环境保护局（USEPA）地下水和饮用水办公室发布 方法524.3（1），“空气中可净化有机化合物的测量 通过毛细管柱气相色谱/质谱法测定水， 2009年8月3日，《联邦公报》（2）第1.0版 该方法用于测定挥发性有机化合物（VOCs） 在成品饮用水中，包括几项重大变化和 对其前身美国环境保护局方法524.2（3）的改进。 本文介绍了优化的仪器操作参数， 包括6分钟的清洗时间和一整套方法验证 数据此处显示的质量控制统计数据包括校准验收 数据、最低报告水平（MRL）、检测限（DLs）和 最低浓度最低报告水平（LCMRL）；二 精度和精度研究，从最初的演示 能力（IDC）；以及实验室试剂空白（LRB）的结果 以及持续校准检查（CCC）样本。包括7个参考文献、表格、图表。

The U.S. Environmental Protection Agency (USEPA) Office of Groundwater and Drinking Water released Method 524.3 (1), "Measurement of Purgeable Organic Compounds in Water by Capillary Column Gas Chromatography/Mass Spectrometry, Revision 1.0," in the Federal Register (2), on August 3, 2009. The new method is used for determination of volatile organic compounds (VOCs) in finished drinking water, and includes several significant changes and improvements over its predecessor, USEPA Method 524.2 (3). This paper presents optimized instrument operating parameters, including a 6-minute purge time, and a complete set of method validation data. Quality control statistics shown here include calibration acceptance data, Minimum Reporting Levels (MRLs), Detection Limits (DLs) and Lowest Concentration Minimum Reporting Levels (LCMRLs); two precision and accuracy studies from the Initial Demonstration of Capability (IDC); and, results from Laboratory Reagent Blanks (LRBs) and Continuing Calibration Check (CCC) samples. Includes 7 references, tables, figures.