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Standard Test Method for Mass Scale Calibration of Thermogravimetric Analyzers 热重分析仪质谱校准的标准测试方法
发布日期: 2019-12-01
1.1 本试验方法描述了热重分析仪质量(或重量)刻度的校准或性能确认,适用于商业和定制仪器。 1.2 以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.3 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 1.4 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 5.1 本试验方法校准或证明了热重仪在环境条件下的一致性。大多数热重分析实验是在温度斜坡条件下或在远离环境条件的等温温度下进行的。本试验方法不涉及温度对质量校准的影响。 5.2 在大多数热重分析实验中,质量变化报告为重量百分比,其中实验过程中任何时间的观察质量除以试样的原始质量。这种报告结果的方法假设仪器的质量规模与质量的增加呈线性关系。 在这种情况下,可能只需要通过与适当的参考进行比较来确认仪器的性能。 5.3 当记录试样的实际质量时,在极少数情况下,可能需要使用校准系数来校正仪器的校准。
1.1 This test method describes the calibration or performance confirmation of the mass (or weight) scale of thermogravimetric analyzers and is applicable to commercial and custom-built apparatus. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method calibrates or demonstrates conformity of thermogravimetric apparatus at ambient conditions. Most thermogravimetry analysis experiments are carried out under temperature ramp conditions or at isothermal temperatures distant from ambient conditions. This test method does not address the temperature effects on mass calibration. 5.2 In most thermogravimetry experiments, the mass change is reported as weight percent in which the observed mass at any time during the course of the experiment is divided by the original mass of the test specimen. This method of reporting results assumes that the mass scale of the apparatus is linear with increasing mass. In such cases, it may be necessary only to confirm the performance of the instrument by comparison to a suitable reference. 5.3 When the actual mass of the test specimen is recorded, the use of a calibration factor to correct the calibration of the apparatus may be required, on rare occasions.
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归口单位: E37.01
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