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Standard Test Method for Volatility Rate by Thermogravimetry 使用热重分析法确定挥发速率的标准测试方法
发布日期: 1999-03-10
1.1本试验方法涵盖了在规定的实验条件下,使用热重分析法在给定温度下评估固体和液体挥发性的程序。该测试方法的结果是以单位时间质量表示的波动率获得的。使用该测试方法可以实现大于或等于5µg/min的速率。 1.2本试验方法的典型温度范围为25°C至500°C。该温度范围可能因使用的仪器而异。 1.3本试验方法旨在通过对单个代表性样品进行热重分析测量,提供样品的挥发性率值。本试验方法的使用者有责任确定满足最终使用要求所需的新鲜样品重复测量的需要和数量。 1.4也可使用与本试验方法等效的基于计算机或电子的仪器、技术或数据处理。 注1-明确建议本试验方法的用户,所有此类仪器或技术可能不是等效的。本试验方法的使用者有责任在使用前确定必要的等效性。 1.5以国际单位制表示的数值应视为标准。 1.6本标准无意解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全和健康实践,并确定监管限制的适用性。
1.1 This test method covers procedures for assessing the volatility of solids and liquids at given temperatures using thermogravimetry under prescribed experimental conditions. Results of this test method are obtained as volatility rates expressed as mass per unit time. Rates > or = to 5 µg/min are achievable with this test method. 1.2 Temperatures typical for this test method are within the range from 25 °C to 500°C. This temperature range may differ depending upon the instrumentation used. 1.3 This test method is intended to provide a value for the volatility rate of a sample using a thermogravimetric analysis measurement on a single representative specimen. It is the responsibility of the user of this test method to determine the need for and the number of repetitive measurements on fresh specimens necessary to satisfy end use requirements. 1.4 Computer- or electronic-based instruments, techniques, or data treatment equivalent to this test method may also be used. Note 1-Users of this test method are expressly advised that all such instruments or techniques may not be equivalent. It is the responsibility of the user of this test method to determine the necessary equivalency prior to use. 1.5 The values stated in SI units are to be regarded as the standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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归口单位: E37.01
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