Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction
水质与灰分;液-液萃取荧光检测高效液相色谱法测定水中15种多环芳烃
发布日期:
2002-08-29
ISO 17993:2002规定了使用带荧光检测的高效液相色谱(HPLC)测定15种选定多环芳烃(PAH)[萘、苊、菲、荧蒽、苯并(a)蒽、苯并(b)荧蒽、苯并(a)芘、二苯并(a,h)蒽、芴、蒽、芘、白杨、苯并(k)荧、茚(1,2,3-cd)芘、苯并(ghi)苝]在饮用水和地下水中的质量浓度大于0005微克/升(每种化合物),以及地表水中的质量浓度大于0,01微克/升。
这种方法经过一些修改后,也适用于废水的分析。该方法可适用于其他多环芳烃,前提是该方法已针对每种情况进行了验证。
ISO 17993:2002 specifies a method using high performance liquid chromatography (HPLC) with fluorescence detection for the determination of 15 selected polycyclic aromatic hydrocarbons (PAH) [naphthalene, acenaphthene, phenanthrene, fluoranthene, benzo(a)anthracene, benzo(b)fluoranthene, benzo(a)pyrene, dibenzo(a,h)anthracene, fluorene, anthracene, pyrene, chrysene, benzo(k)fluoranthene, indeno(1,2,3-cd)pyrene, benzo(ghi)perylene] in drinking and ground water in mass concentrations greater than 0,005 microgram/litre (for each single compound) and surface waters in mass concentrations above 0,01 microgram/litre.
This method is, with some modification, also suitable for the analysis of waste water. This method may be applicable to other PAH, provided the method is validated for each case.