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历史 ASTM E1683-02(2014)e1
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Standard Practice for Testing the Performance of Scanning Raman Spectrometers 扫描拉曼光谱仪性能的标准实践
发布日期: 2014-05-01
1.1本规程涵盖扫描拉曼光谱仪性能的常规测试,并在性能下降时协助定位问题。它还旨在作为获取和报告拉曼光谱的指南。 1.2以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.3 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全和健康实践,并确定监管限制的适用性。 具体注意事项见7.2.1。 1.4由于使用激光存在重大危险,因此应结合本实践遵守ANSI Z136.1。 ====意义和用途====== 4.1应定期检查扫描拉曼光谱仪,以确定其条件是否足以进行常规测量或是否已发生变化。本规程旨在促进确定,如果性能不符合要求,则确定需要注意的系统部分。这些测试适用于商用的单、双或三单色扫描拉曼仪器。它们不适用于多通道或傅立叶变换仪器,或需要脉冲激光源的门控积分器系统。 本规程仅适用于经过培训的光学光谱仪,应与标准文本结合使用。
1.1 This practice covers routine testing of scanning Raman spectrometer performance and to assist in locating problems when performance has degraded. It is also intended as a guide for obtaining and reporting Raman spectra. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautions, see 7.2.1. 1.4 Because of the significant dangers associated with the use of lasers, ANSI Z136.1 should be followed in conjunction with this practice. ====== Significance And Use ====== 4.1 A scanning Raman spectrometer should be checked regularly to determine if its condition is adequate for routine measurements or if it has changed. This practice is designed to facilitate that determination and, if performance is unsatisfactory, to identify the part of the system that needs attention. These tests apply for single-, double-, or triplemonochromator scanning Raman instruments commercially available. They do not apply for multichannel or Fourier transform instruments, or for gated integrator systems requiring a pulsed laser source. Use of this practice is intended only for trained optical spectroscopists and should be used in conjunction with standard texts.
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归口单位: E13.08
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