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Standard Test Method for Radiochemical Determination of Uranium Isotopes in Soil by Alpha Spectrometry 通过Alpha光谱法测定土壤中铀同位素的标准测试方法
发布日期: 2019-11-01
1.1 本试验方法包括测定土壤中发射α的铀同位素。本试验方法描述了一种测定土壤中铀同位素的可接受方法。 2. 1.2 该测试方法旨在分析10 g土壤。该试验方法可能无法完全溶解土壤基质中的所有形式的铀。研究表明,使用氢氟酸溶解土壤的结果比使用熔融全溶解的结果低。 1.3 检测下限取决于计数时间、样本量、检测器、背景和示踪剂产量。化学产率平均为78 % 在单个实验室评估中,以及66 % 在一项实验室间合作研究中。 1.4 以国际单位制表示的数值应视为标准值。括号中给出的值仅供参考。 1.5 本标准并非旨在解决与其使用相关的所有安全问题(如有)。 本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 第节给出了具体的预防说明 11 . 1.6 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 5.1 本试验方法用于分析土壤中的α放射性铀同位素。它可用于确定基准铀水平和监测核设施的沉积。
1.1 This test method covers the determination of alpha-emitting uranium isotopes in soil. This test method describes one acceptable approach to the determination of uranium isotopes in soil. 2 1.2 The test method is designed to analyze 10 g of soil. This test method may not be able to completely dissolve all forms of uranium in the soil matrix. Studies have indicated that the use of hydrofluoric acid to dissolve soil has resulted in lower values than results using total dissolution by fusion. 1.3 The lower limit of detection is dependent on count time, sample size, detector, background, and tracer yield. The chemical yield averaged 78 % in a single laboratory evaluation, and 66 % in an interlaboratory collaborative study. 1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 11 . 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method is used to analyze soil for alpha-emitting uranium isotopes. It can be used to establish baseline uranium levels and to monitor depositions from nuclear facilities.
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归口单位: C26.05
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