1.1 本试验方法包括在0.0007范围内测定镍、镍铁和镍合金中的磷 % 至0.05 %. 1.2 砷、铬、铪、铌、硅、钽、钛和钨干扰，但可以通过络合或挥发（铬）来避免干扰。最低磷含量（0.0007 %) 只能在干扰元素含量低的样品中达到。 1.3 以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.4 本标准并非旨在解决与其使用相关的所有安全问题（如有）。本标准的用户有责任在使用前制定适当的安全、健康和环境实践，并确定监管限制的适用性。 有关使用本试验方法的具体危险，请参阅实践 E50 . 请参阅本试验方法中给出的具体警告注释。 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒（TBT）委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 5.1 本试验方法用于通过分子吸收光谱法测定镍、镍铁和镍合金样品中的磷，以检查是否符合成分规范。 假设所有使用该程序的人都是经过培训的分析员，能够熟练、安全地执行常见的实验室程序。预计工作将在配备适当的实验室中进行，并遵循适当的废物处理程序。必须遵循适当的质量控制实践，如指南中所述 E882 .

1.1 This test method covers the determination of phosphorus in nickel, ferronickel, and nickel alloys in the range 0.0007 % to 0.05 %. 1.2 Arsenic, chromium, hafnium, niobium, silicon, tantalum, titanium, and tungsten interfere, but the interference can be avoided by complexation or volatilization (for chromium). The lowest phosphorus content (0.0007 %) can be reached only in samples with low contents of interfering elements. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazards associated with the use of this test method see Practices E50 . Refer to specific warning notes given throughout this test method. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 This test method is used for the determination of phosphorus in nickel, ferronickel, and nickel alloy samples by molecular absorption spectrometry to check compliance with compositional specifications. It is assumed that all who use the procedure will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that the work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed, such as those described in Guide E882 .