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现行 ASTM D3326-07(2024)
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Standard Practice for Preparation of Samples for Identification of Waterborne Oils 鉴定水性油样品制备的标准实施规程
发布日期: 2024-04-01
1.1 本规程涵盖了从水中回收的水性油的分析准备工作。鉴定是基于水性油与可疑来源油的物理和化学特性的比较。这些油可能来源于石油或植物/动物,或两者兼而有之。七个程序如下: 小节 程序A(适用于50个以上的样品 mL体积,含有大量沸点高于280的碳氢化合物 °C) 8. 到 12 程序B(适用于含有大量沸点高于280的碳氢化合物的样品 °C) 13 到 17 步骤C(对于含有大量沸点低于280的组分的水性油 °C以及这些成分和更高沸点成分的混合物) 18 到 22 程序D(适用于同时含有石油和植物/动物油的样品) 23 到 27 程序E(适用于轻质原油和中等馏分燃料的样品) 28 到 34 步骤F(适用于水上油薄膜) 35 到 39 步骤G(适用于浸油样品) 40 到 44 1.2 《实施规程》中描述了水性油样品的分析检验程序 D3415 和试验方法 D3328 , D3414 和 D3650 。有关所选样品制备方法,请参阅单独的油鉴定测试方法。在选择最佳方法时,应考虑样品制备方法的脱沥青效果。 1.3 以国际单位制表示的数值应视为标准。 本标准不包括其他计量单位。 1.4 本标准并不旨在解决与其使用相关的所有安全问题(如有)。本标准的使用者有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 第节中给出了具体的警告声明 6. 和 32 . 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认的标准化原则制定的。 ====意义和用途====== 4.1 回收油的识别是通过与已知油的比较来确定的,因为已知油可能与特定的回收油有关,例如可疑或可疑来源。因此,必须收集此类已知油的样本,并将其与未知油一起提交分析。在没有直接匹配的情况下,即仅通过分析库,不太可能单独识别未知石油的来源。
1.1 This practice covers the preparation for analysis of waterborne oils recovered from water. The identification is based upon the comparison of physical and chemical characteristics of the waterborne oils with oils from suspect sources. These oils may be of petroleum or vegetable/animal origin, or both. Seven procedures are given as follows: Sections Procedure A (for samples of more than 50 mL volume containing significant quantities of hydrocarbons with boiling points above 280 °C) 8 to 12 Procedure B (for samples containing significant quantities of hydrocarbons with boiling points above 280 °C) 13 to 17 Procedure C (for waterborne oils containing significant amounts of components boiling below 280 °C and to mixtures of these and higher boiling components) 18 to 22 Procedure D (for samples containing both petroleum and vegetable/animal derived oils) 23 to 27 Procedure E (for samples of light crudes and medium distillate fuels) 28 to 34 Procedure F (for thin films of oil-on-water) 35 to 39 Procedure G (for oil-soaked samples) 40 to 44 1.2 Procedures for the analytical examination of the waterborne oil samples are described in Practice D3415 and Test Methods D3328 , D3414 , and D3650 . Refer to the individual oil identification test methods for the sample preparation method of choice. The deasphalting effects of the sample preparation method should be considered in selecting the best methods. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific caution statements are given in Sections 6 and 32 . 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 4.1 Identification of a recovered oil is determined by comparison with known oils selected because of their possible relationship to the particular recovered oil, for example, suspected or questioned sources. Thus, samples of such known oils must be collected and submitted along with the unknown for analysis. It is unlikely that identification of the sources of an unknown oil by itself can be made without direct matching, that is, solely with a library of analyses.
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归口单位: D19.06
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