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Standard Test Method for Analysis of Acrylonitrile by Gas Chromatography 用气相色谱法分析丙烯腈的标准试验方法
发布日期: 2018-10-01
1.1 本试验方法包括通过火焰离子化检测器气相色谱法测定丙烯腈中的杂质和纯度。适用于99至100范围内的丙烯腈 % 纯洁 1.2 以国际单位制表示的数值应视为标准值。括号中给出的值仅供参考。 1.3 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 具体危险说明见第节 6. 和 7. . 1.4 查看当前MSDS,了解有关毒性、急救程序和安全预防措施的详细信息。 1.5 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 4.1 本试验方法旨在根据丙烯腈中通常存在的杂质获得丙烯腈纯度,并可用于最终产品检验和过程控制。 4.2 本试验方法将测量以下杂质:丙酮、丙烯醛、乙腈和乙醛。它还允许校准其他杂质,包括苯、甲基丙烯腈、恶唑、丙腈、顺式- 巴豆腈、反式巴豆腈和其他有特定杂质标准的物质。
1.1 This test method covers the determination of the impurities in, and the purity of, acrylonitrile by flame ionization detector gas chromatography. It is applicable to acrylonitrile in the range of 99 to 100 % purity. 1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Sections 6 and 7 . 1.4 Review the current MSDS for detailed information concerning toxicity, first aid procedures, and safety precautions. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 4.1 This test method is designed to obtain acrylonitrile purity on the basis of impurities normally present in acrylonitrile and may be useful for final product inspection and process control. 4.2 This test method will measure the following impurities: acetone, acrolein, acetonitrile, and acetaldehyde. It also will allow calibration of other impurities including benzene, methacrylonitrile, oxazole, propionitrile, cis-crotononitrile, trans-crotononitrile, and others where specific impurity standards are available.
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归口单位: D20.15
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