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Standard Test Methods of Chemical Analysis of Sulfonated and Sulfated Oils 磺化和硫酸化油的化学分析标准试验方法
发布日期: 2016-07-01
1.1 这些试验方法包括磺化油和硫酸化油的化学分析。分析程序按以下顺序出现: 部分 湿度: 试验方法A.用挥发性溶剂蒸馏水 4 – 9 试验方法B.热板法测定水分和挥发物 10 – 14 有机结合的硫酸酐: 试验方法A.滴定试验 15 – 19 试验方法B.萃取滴定试验 20 – 24 试验方法C.灰分重量试验(在真实存在的情况下 磺酸盐) 25 – 28 总脱硫脂肪物质 29 – 32 总活性成分 33 – 36 不皂化非挥发性物质 37 – 41 无机盐 42 – 46 总碱度 47 – 49 总氨 50 – 52 以游离脂肪酸或酸值表示的酸度: 试验方法A.在没有铵或三乙醇胺皂的情况下 53 – 56 试验方法B 无铵或三乙醇胺皂(盐水试验) 57 – 60 试验方法C.在铵或三乙醇胺皂存在下 61 – 63 水不溶性有机溶剂与蒸汽挥发 64 – 70 1.2 以英寸表示的值- 磅单位应视为标准。英寸-磅单位的公制等价物可能是近似值。 1.3 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全和健康实践,并确定监管限制的适用性。 试剂和材料有材料安全数据表。使用前检查其危险性。
1.1 These test methods cover the chemical analysis of sulfonated and sulfated oils. The analytical procedures appear in the following order: Section Moisture: Test Method A. Water by Distillation with Volatile Solvent 4 – 9 Test Method B. Moisture and Volatile Matter by Hot-Plate Method 10 – 14 Organically Combined Sulfuric Anhydride: Test Method A. Titration Test 15 – 19 Test Method B. Extraction-Titration Test 20 – 24 Test Method C. Ash-Gravimetric Test (in the Presence of True Sulfonates) 25 – 28 Total Desulfated Fatty Matter 29 – 32 Total Active Ingredients 33 – 36 Unsaponifiable Nonvolatile Matter 37 – 41 Inorganic Salts 42 – 46 Total Alkalinity 47 – 49 Total Ammonia 50 – 52 Acidity as Free Fatty Acids or Acid Number: Test Method A. In the Absence of Ammonium or Triethanolamine Soaps 53 – 56 Test Method B. In the Presence of Dark Colored Oils but in the Absence of Ammonium or Triethanolamine Soaps (Brine Test) 57 – 60 Test Method C. In the Presence of Ammonium or Triethanolamine Soaps 61 – 63 Water-Immiscible Organic Solvents Volatile with Steam 64 – 70 1.2 The values stated in inch-pound units are to be regarded as the standard. The metric equivalents of inch-pound units may be approximate. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.
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归口单位: D12.12
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