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历史 ASTM D7417-17
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Standard Test Method for Analysis of In-Service Lubricants Using Particular Four-Part Integrated Tester (Atomic Emission Spectroscopy, Infrared Spectroscopy, Viscosity, and Laser Particle Counter) 使用特殊的四部分集成测试仪(原子发射光谱 红外光谱 粘度和激光粒子计数器)分析使用中润滑剂的标准测试方法
发布日期: 2017-10-01
1.1 该测试方法包括使用自动测试设备对在用润滑剂进行定量分析,该设备集成了以下各种技术:原子发射光谱法、红外光谱法、粘度和颗粒计数。 1.2 这适用于粘度在ISO 10和ISO 320之间且性能在中给出的范围内的在用润滑油 表1和 2. . 表1测量、计算和报告的元件测试参数 要素 低范围,mg/kg 高范围,mg/kg 要素 低范围,mg/kg 高范围,mg/kg 铝 5至100 不适用 钼 10至1000 不适用 钡 25至150 150至2000 镍 5至100 不适用 硼 5至100 100至1000 磷 100至600 600至4000 钙 25至500 500至9000 钾 10至1000 1000至4000 铬 8至100 不适用 硅 5至150 150至3000 铜 5至500 500至1000 钠 10至1000 不适用 铁 6至1000 1000至3000 锡 6至100 不适用 领导 6至150 不适用 钛 8至100 不适用 镁 5至100 100至3000 钒 7至100 不适用 锰 5至100 不适用 锌 8至100 100至4000 表2测量、计算和报告的物理特性参数 注1: 审查测试方法 D4739 和 D2896 用于特殊润滑油应用。 物理性质 范围 水 % 按质量计 0.1至3 乙二醇, % 按质量计 0.1到2 烟灰 % 按质量计 0.1至4 燃料稀释, % 按质量计 0.1至15 氧化,abs。 0.1至50 硝化,abs。 0.1至35 计算粘度-IR 4至35(100°cSt) 粘度40 °C,cSt(可选) 30至320 粘度100 °C,cSt(可选) 5至25 粘度指数 5至150 碱值,mg/g KOH 1.0至17 1.3 该试验方法可用于确定在用润滑剂的磨损和污染趋势,并且可能不会给出与当前ASTM试验方法相同的数值结果。 1.4 本试验方法不适用于原油。 1.5 以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.6 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 (第节给出了具体的危险说明。) 9 和 11.3 .) 1.7 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 5.1 集成测试仪主要用于对汽车、公路卡车运输、采矿、建筑、越野“采矿”、海洋、工业、发电、农业和制造业中使用的在用润滑油进行现场分析。 5.2 在进行主动预防性维护时,运行中润滑剂的即时分析结果至关重要。现场油分析与这些程序结合使用时,允许连续系统监测和污染控制,从而潜在地提高设备的“运行时间”和设备寿命。
1.1 This test method covers the quantitative analysis of in-service lubricants using an automatic testing device that integrates these varied technologies: atomic emission spectroscopy, infrared spectroscopy, viscosity, and particle counting. 1.2 This is suited for in-service lubricating oils having viscosities in the range between ISO 10 and ISO 320 and properties in the ranges given in Tables 1 and 2 . TABLE 1 Element Test Parameters Measured, Calculated, and Reported Element Low Range, mg/kg High Range, mg/kg Element Low Range, mg/kg High Range, mg/kg Aluminum 5 to 100 NA Molybdenum 10 to 1000 NA Barium 25 to 150 150 to 2000 Nickel 5 to 100 NA Boron 5 to 100 100 to 1000 Phosphorous 100 to 600 600 to 4000 Calcium 25 to 500 500 to 9000 Potassium 10 to 1000 1000 to 4000 Chromium 8 to 100 NA Silicon 5 to 150 150 to 3000 Copper 5 to 500 500 to 1000 Sodium 10 to 1000 NA Iron 6 to 1000 1000 to 3000 Tin 6 to 100 NA Lead 6 to 150 NA Titanium 8 to 100 NA Magnesium 5 to 100 100 to 3000 Vanadium 7 to 100 NA Manganese 5 to 100 NA Zinc 8 to 100 100 to 4000 TABLE 2 Physical Properties Parameters Measured, Calculated, and Reported Note 1: Review Test Method D4739 and D2896 for particular lubricating oil applications. Physical Property Range Water,  % by mass 0.1 to 3 Glycol,  % by mass 0.1 to 2 Soot,  % by mass 0.1 to 4 Fuel Dilution,  % by mass 0.1 to 15 Oxidation, abs. 0.1 to 50 Nitration, abs. 0.1 to 35 Calculated Viscosity - IR 4 to 35 (100° cSt) Viscosity 40 °C, cSt (optional) 30 to 320 Viscosity 100 °C, cSt (optional) 5 to 25 Viscosity Index 5 to 150 Base Number, mg/g KOH 1.0 to 17 1.3 This test method may be used to establish trends in wear and contamination of in-service lubricants and may not give equivalent numerical results to current ASTM test methods. 1.4 This test method is not intended for use with crude oil. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Specific hazard statements are given in Section 9 and 11.3 .) 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 5.1 The integrated tester is primarily used to perform on-site analysis of in-service lubricants used in the automotive, highway trucking, mining, construction, off-road “mining,” marine, industrial, power generation, agriculture, and manufacturing industries. 5.2 The immediate results of analysis of in-service lubricants are critical when performing proactive and preventative maintenance. On-site oil analysis, when used in conjunction with these programs, allows continuous system monitoring and contamination control potentially improving equipment “up-time” and equipment life.
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归口单位: D02.96.07
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