首页 馆藏资源 舆情信息 标准服务 科研活动 关于我们
现行 ASTM D4047-18
到馆提醒
收藏跟踪
购买正版
Standard Test Method for Phosphorus in Lubricating Oils and Additives by Quinoline Phosphomolybdate Method 用喹啉磷钼酸盐法测定润滑油和添加剂中磷的标准试验方法
发布日期: 2018-04-01
1.1 本试验方法涵盖0.005的测定 % 至10.0 % 按未使用的润滑油和添加剂浓缩物中的磷质量计。没有理由怀疑其对过滤后的旧润滑油的适用性,但尚未对此应用进行系统研究。 1.2 本试验方法适用于正常使用中含有任何磷化合物的样品。 注1: 本试验方法扩展了IP 149先前版本的范围,并取代IP 148和IP 149先前版本作为参考方法。 1.3 本试验方法不受大多数干扰,因为喹啉磷钼酸盐沉淀物的高不溶性导致成分恒定,并且不受大多数吸附或封闭杂质的影响,特别是不受阳离子的影响,否则会干扰沉淀物的后续滴定。 1.4 钡、钙、镁、锌、铁、铝、碱盐、柠檬酸和柠檬酸盐、磷含量高达18倍的铬和高达3.5倍的钛不会干扰试验方法。 1.5 以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。 1.6 本标准并非旨在解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全、健康和环境实践,并确定监管限制的适用性。 有关具体的危险说明,请参阅 6. 9 . 1.7 本国际标准是根据世界贸易组织技术性贸易壁垒(TBT)委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。 ====意义和用途====== 4.1 有关润滑油或添加剂中磷含量以及含磷添加剂的知识可用于预测性能特征。
1.1 This test method covers the determination of 0.005 % to 10.0 % by mass phosphorus in unused lubricating oil and additive concentrates. There is no reason to doubt its applicability to filtered, used lubricating oils, but no systematic study of this application has been made. 1.2 The test method is applicable to samples containing any of the phosphorus compounds in normal use. Note 1: This test method extends the scope of the previous version of IP 149 and replaces IP 148 and the previous version of IP 149 as a referee method. 1.3 This test method is free from most interferences because the high insolubility of the quinoline phosphomolybdate precipitate leads to constant composition and freedom from most adsorbed or occluded impurities, especially from cations which would otherwise interfere in the subsequent titration of the precipitate. 1.4 Barium, calcium, magnesium, zinc, iron, aluminum, alkali salts, citric acid and citrates, chromium up to 18 times the phosphorus content, and titanium up to 3.5 times do not interfere with the test method. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 6.9 . 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ====== 4.1 Knowledge of the phosphorus content, and thus the phosphorus-containing additives, in a lubricating oil or additive can be used to predict performance characteristics.
分类信息
关联关系
研制信息
归口单位: D02.03
相似标准/计划/法规
现行
GOST R 52240-2004
Масла смазочные и присадки. Методы определения фосфора
润滑油和添加剂 磷测试方法
现行
ASTM D874-23
Standard Test Method for Sulfated Ash from Lubricating Oils and Additives
润滑油和添加剂中硫酸盐灰分的标准试验方法
2023-03-01
现行
BS 2000-149-1993
Methods of test for petroleum and its products-Petroleum products. Lubricating oils and additives. Determination of phosphorus content. Quinoline phosphomolybdate method
石油及其产品的试验方法 石油产品 润滑油和添加剂 磷含量的测定 喹啉磷钼酸盐法
1993-02-28
现行
ASTM D7751-16(2021)
Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
用EDXRF分析法测定润滑油中添加剂元素的标准试验方法
2021-07-01
现行
SH/T 0749-2004
润滑油及添加剂中添加元素含量测定法(电感耦合等离子体发射光谱法)
Standard test method for determination of additive elements in both lubricating oils and additives by inductively coupled plasma atomic emission spectrometry
2004-04-09
现行
ASTM D7546-24
Standard Test Method for Determination of Moisture in New and In-Service Lubricating Oils and Additives by Relative Humidity Sensor
用相对湿度传感器测定新的和使用中的润滑油和添加剂中水分的标准试验方法
2024-02-01
现行
GB/T 11133-2015
石油产品、润滑油和添加剂中水含量的测定 卡尔费休库仑滴定法
Standard test method for determination of water in petroleum products, lubricating oils and additives—Coulometric Karl Fischer titration method
2015-12-31
现行
ASTM D6304-20
Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration
通过库仑卡尔费休滴定测定石油产品 润滑油和添加剂中的水的标准测试方法
2020-12-01
现行
ASTM D4951-14(2019)
Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
用电感耦合等离子体原子发射光谱法测定润滑油中添加剂元素的标准试验方法
2019-12-01
现行
NB/SH/T 0824-2010
润滑油中添加剂元素含量的测定 电感耦合等离子体原子发射光谱法
Standard test method for determination of additive elements in lubricating oils by inductively coupled plasma atomic emission spectrometry
2010-05-01
现行
NB/SH/T 0822-2010
润滑油中磷、硫、钙和锌含量的测定 能量色散X射线荧光光谱法
Standard test method for determination of phosphorus,sulfur,calcium,and zinc in lubrication oils by energy dispersive X-ray fluorescence spectroscopy
2010-05-01
现行
ASTM D6481-24
Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy
用能量分散X射线荧光光谱法测定润滑油中磷、硫、钙和锌的标准试验方法
2024-03-01
现行
ASTM D893-14(2018)
Standard Test Method for Insolubles in Used Lubricating Oils
使用润滑油不溶物的标准试验方法
2018-10-01
现行
ASTM D892-23
Standard Test Method for Foaming Characteristics of Lubricating Oils
润滑油发泡特性的标准试验方法
2023-10-01
现行
ASTM D2711-22
Standard Test Method for Demulsibility Characteristics of Lubricating Oils
润滑油破乳化特性的标准试验方法
2022-11-01
现行
GB/T 8926-2012
在用的润滑油不溶物测定法
Standard test method for insolubles in used lubricating oils
2012-11-05
现行
ASTM D91-24
Standard Test Method for Precipitation Number of Lubricating Oils
润滑油沉淀值的标准试验方法
2024-11-01
现行
ASTM D6443-24
Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure)
用波长分散X射线荧光光谱法测定未使用的润滑油和添加剂中钙、氯、铜、镁、磷、硫和锌的标准试验方法(数学校正程序)
2024-05-01
现行
NB/SH/T 0880-2014
润滑油及添加剂中的钙、氯、铜、镁、磷、硫和锌含量的测定 波长色散X射线荧光光谱法
Standard test method for determination of calcium,chlorine,copper,magnesium,phosphorus,sulfur,and zinc in unused lubricating oils and additives by wavelength dispersive X-ray fluorescence spectrometry (mathematical correction procedure)
2014-06-29
现行
ASTM D4927-20
Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy
用波长色散X射线荧光光谱法对润滑剂和添加剂成分进行元素分析的标准试验方法钡钙磷硫锌
2020-12-01